Technology Process of C31H26FN3O8
There total 9 articles about C31H26FN3O8 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C24H21FN2O8;
With
dmap; Triphenylsilyl chloride; triethylamine;
In
acetonitrile;
at 20 ℃;
for 14h;
With
ammonia;
In
tetrahydrofuran; acetonitrile;
at 20 ℃;
for 2h;
benzoyl chloride;
With
pyridine;
at 20 ℃;
for 16h;
- Guidance literature:
-
With
pyridine;
at 20 ℃;
for 16h;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: triphenylphosphine; pyridine; 1H-imidazole; iodine / tetrahydrofuran / 14 h / 0 - 20 °C
2.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 6 h / 0 - 60 °C
3.1: iodine; lead(II) carbonate / 0 - 20 °C
4.1: pyridine / 10 h / 0 - 20 °C
5.1: 15-crown-5 / N,N-dimethyl-formamide / 3 h / 60 - 70 °C
6.1: Triphenylsilyl chloride; dmap; triethylamine / acetonitrile / 14 h / 20 °C
6.2: 2 h / 20 °C
6.3: 16 h / 20 °C
With
pyridine; 1H-imidazole; dmap; lead(II) carbonate; 15-crown-5; Triphenylsilyl chloride; iodine; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; triphenylphosphine;
In
tetrahydrofuran; N,N-dimethyl-formamide; acetonitrile;