methyl 2-[(1-benzyloxyallyl)-(4-nitrobenzenesulfonyl)amino]-(S)-pent-4-enoate

Base Information

Chemical Name:methyl 2-[(1-benzyloxyallyl)-(4-nitrobenzenesulfonyl)amino]-(S)-pent-4-enoate
CAS No.:282527-06-4
Molecular Formula:C₂₂H₂₄N₂O₇S
Molecular Weight:460.508
Hs Code.:

Synonyms:methyl 2-[(1-benzyloxyallyl)-(4-nitrobenzenesulfonyl)amino]-(S)-pent-4-enoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 2-[(1-benzyloxyallyl)-(4-nitrobenzenesulfonyl)amino]-(S)-pent-4-enoate

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of methyl 2-[(1-benzyloxyallyl)-(4-nitrobenzenesulfonyl)amino]-(S)-pent-4-enoate

There total 1 articles about methyl 2-[(1-benzyloxyallyl)-(4-nitrobenzenesulfonyl)amino]-(S)-pent-4-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 67515-49-5
1-benzyloxyallene

: methyl (S)-2-(4-nitrobenzenesulfonylamino)pent-4-enoate

: 282527-06-4
methyl 2-[(1-benzyloxyallyl)-(4-nitrobenzenesulfonyl)amino]-(S)-pent-4-enoate

Guidance literature:: With 1,3-bis-(diphenylphosphino)propane; triethylamine; palladium diacetate; In acetonitrile; at 20 ℃; for 1h;
DOI:10.1039/b001253j

Reference yield: 90.0%

: 282527-06-4
methyl 2-[(1-benzyloxyallyl)-(4-nitrobenzenesulfonyl)amino]-(S)-pent-4-enoate

: 282527-08-6
methyl (2S)-6-benzyloxy-1-(4-nitrobenzenesulfonyl)-1,2,3,6-tetrahydropyridine-2-carboxylate

Guidance literature:: Grubbs catalyst first generation; In dichloromethane; at 20 ℃;
DOI:10.1039/b001253j

Reference yield:

: 282527-06-4
methyl 2-[(1-benzyloxyallyl)-(4-nitrobenzenesulfonyl)amino]-(S)-pent-4-enoate

: 282527-10-0
methyl (S,S)-6-allyl-1-(4-nitrobenzenesulfonyl)-1,2,3,6-tetrahydropyridine-2-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / RuCl₂[PCy₃]2[=CHPh] / CH₂Cl₂ / 16 h / 20 °C

2: 100 percent / BF₃*OEt₂ / CH₂Cl₂ / 4 h / -78 °C

With boron trifluoride diethyl etherate; Grubbs catalyst first generation; In dichloromethane;
DOI:10.1002/1615-4169(200208)344:6/7<736::AID-ADSC736>3.0.CO;2-8