(2R,3R)-3-(3-methoxyphenyl)-N,N,2-trimethylpent-4-eneamide

Base Information

Chemical Name:(2R,3R)-3-(3-methoxyphenyl)-N,N,2-trimethylpent-4-eneamide
CAS No.:1367879-30-8
Molecular Formula:C₁₅H₂₁NO₂
Molecular Weight:247.337
Hs Code.:

Synonyms:(2R,3R)-3-(3-methoxyphenyl)-N,N,2-trimethylpent-4-eneamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R,3R)-3-(3-methoxyphenyl)-N,N,2-trimethylpent-4-eneamide

Chemical Property:

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Technology Process of (2R,3R)-3-(3-methoxyphenyl)-N,N,2-trimethylpent-4-eneamide

There total 4 articles about (2R,3R)-3-(3-methoxyphenyl)-N,N,2-trimethylpent-4-eneamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6099-04-3,17570-26-2
trans-3-methoxycinnamic acid

: 1367879-30-8
(2R,3R)-3-(3-methoxyphenyl)-N,N,2-trimethylpent-4-eneamide

Guidance literature:: Multi-step reaction with 7 steps

1.1: diisobutylaluminium hydride / toluene / -15 - 20 °C / Inert atmosphere

1.2: Cooling with ice

2.1: carbon tetrabromide / 10 h / 60 °C

3.1: triethylamine; lithium hexamethyldisilazane / toluene / 2.83 h / -60 °C / Inert atmosphere

3.2: 0.17 h

3.3: Cooling with ice

4.1: ethanol; tert-butyl methyl ether / 10 °C / Resolution of racemate

5.1: hydrogenchloride / ethyl acetate; water / 0.25 h / 20 °C

6.1: thionyl chloride / toluene / 4 h / 90 °C

7.1: triethylamine / dichloromethane / 1 h / 20 °C / Cooling with ice

With hydrogenchloride; thionyl chloride; diisobutylaluminium hydride; triethylamine; lithium hexamethyldisilazane; carbon tetrabromide; In ethanol; dichloromethane; tert-butyl methyl ether; water; ethyl acetate; toluene;

Reference yield:

: 125617-35-8
(E)-3-(3-Methoxyphenyl)-2-propen-1-ol

: 1367879-30-8
(2R,3R)-3-(3-methoxyphenyl)-N,N,2-trimethylpent-4-eneamide

Guidance literature:: Multi-step reaction with 6 steps

1.1: carbon tetrabromide / 10 h / 60 °C

2.1: triethylamine; lithium hexamethyldisilazane / toluene / 2.83 h / -60 °C / Inert atmosphere

2.2: 0.17 h

2.3: Cooling with ice

3.1: ethanol; tert-butyl methyl ether / 10 °C / Resolution of racemate

4.1: hydrogenchloride / ethyl acetate; water / 0.25 h / 20 °C

5.1: thionyl chloride / toluene / 4 h / 90 °C

6.1: triethylamine / dichloromethane / 1 h / 20 °C / Cooling with ice

With hydrogenchloride; thionyl chloride; triethylamine; lithium hexamethyldisilazane; carbon tetrabromide; In ethanol; dichloromethane; tert-butyl methyl ether; water; ethyl acetate; toluene;

Reference yield:

: 1384457-47-9
(2R,3R)-3-(3-methoxyphenyl)-2-methylpent-4-enoic acid (R)-1-phenylethylamine salt

: 1367879-30-8
(2R,3R)-3-(3-methoxyphenyl)-N,N,2-trimethylpent-4-eneamide

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride / ethyl acetate; water / 0.25 h / 20 °C

2: thionyl chloride / toluene / 4 h / 90 °C

3: triethylamine / dichloromethane / 1 h / 20 °C / Cooling with ice

With hydrogenchloride; thionyl chloride; triethylamine; In dichloromethane; water; ethyl acetate; toluene;