methyl{[2'-(3''-phenylprop-1''-ynyl)cyclohept-1'-en-1'-yl]methylene}amine N-oxide

Base Information

Chemical Name:methyl{[2'-(3''-phenylprop-1''-ynyl)cyclohept-1'-en-1'-yl]methylene}amine N-oxide
CAS No.:863498-67-3
Molecular Formula:C₁₈H₂₁NO
Molecular Weight:267.371
Hs Code.:

Synonyms:methyl{[2'-(3''-phenylprop-1''-ynyl)cyclohept-1'-en-1'-yl]methylene}amine N-oxide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl{[2'-(3''-phenylprop-1''-ynyl)cyclohept-1'-en-1'-yl]methylene}amine N-oxide

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Technology Process of methyl{[2'-(3''-phenylprop-1''-ynyl)cyclohept-1'-en-1'-yl]methylene}amine N-oxide

There total 3 articles about methyl{[2'-(3''-phenylprop-1''-ynyl)cyclohept-1'-en-1'-yl]methylene}amine N-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 863498-63-9
2-(3'-phenylprop-1'-ynyl)cyclohept-1-ene-1-carbaldehyde

: 4229-44-1
N-methylhydroxyamine hydrochloride

: 863498-67-3
methyl{[2'-(3''-phenylprop-1''-ynyl)cyclohept-1'-en-1'-yl]methylene}amine N-oxide

Guidance literature:: With sodium acetate; In dichloromethane; at 20 ℃; for 7h;
DOI:10.1002/ejoc.200400922

Reference yield:

: 10147-11-2
propargyl benzene

: 863498-67-3
methyl{[2'-(3''-phenylprop-1''-ynyl)cyclohept-1'-en-1'-yl]methylene}amine N-oxide

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / CuI; NEt₃ / PdCl₂(PPh₃)2 / benzene / 9 h / 20 °C

2: 57 percent / NaOAc / CH₂Cl₂ / 7 h / 20 °C

With copper(l) iodide; sodium acetate; triethylamine; bis-triphenylphosphine-palladium(II) chloride; In dichloromethane; benzene; 1: Sonogashira reaction;
DOI:10.1002/ejoc.200400922

Reference yield:

: 85236-13-1
2-bromocyclohept-1-ene-1-carbaldehyde

: 863498-67-3
methyl{[2'-(3''-phenylprop-1''-ynyl)cyclohept-1'-en-1'-yl]methylene}amine N-oxide

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / CuI; NEt₃ / PdCl₂(PPh₃)2 / benzene / 9 h / 20 °C

2: 57 percent / NaOAc / CH₂Cl₂ / 7 h / 20 °C

With copper(l) iodide; sodium acetate; triethylamine; bis-triphenylphosphine-palladium(II) chloride; In dichloromethane; benzene; 1: Sonogashira reaction;
DOI:10.1002/ejoc.200400922