6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-2-(2-methylphenyl)benzoxazole

Base Information

Chemical Name:6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-2-(2-methylphenyl)benzoxazole
CAS No.:1325241-74-4
Molecular Formula:C₂₀H₂₂BNO₃
Molecular Weight:335.211
Hs Code.:

Synonyms:6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-2-(2-methylphenyl)benzoxazole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-2-(2-methylphenyl)benzoxazole

Chemical Property:

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Technology Process of 6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-2-(2-methylphenyl)benzoxazole

There total 2 articles about 6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-2-(2-methylphenyl)benzoxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1226074-81-2
6-bromo-2-(2-methylphenyl)benzoxazole

: 73183-34-3
bis(pinacol)diborane

: 1325241-74-4
6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-2-(2-methylphenyl)benzoxazole

Guidance literature:: With C₃₆H₄₉ClFeNPPd; potassium acetate; In 1,4-dioxane; at 80 ℃; for 6h; Inert atmosphere;
DOI:10.1016/j.tet.2011.06.057

Reference yield:

: 32959-60-7
2-(2-methylphenyl)-1,3-benzoxazole

: 1325241-74-4
6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-2-(2-methylphenyl)benzoxazole

Guidance literature:: Multi-step reaction with 2 steps

1: N-Bromosuccinimide; {(Pd{Fe(η5-C5H5)(η5-C5H3C(CH3)=NPh)}(μ-Cl))2}; acetic acid / 8 h / 100 °C

2: C₃₆H₄₉ClFeNPPd; potassium acetate / 1,4-dioxane / 6 h / 80 °C / Inert atmosphere

With N-Bromosuccinimide; {(Pd{Fe(η5-C5H5)(η5-C5H3C(CH3)=NPh)}(μ-Cl))2}; C₃₆H₄₉ClFeNPPd; potassium acetate; acetic acid; In 1,4-dioxane;
DOI:10.1016/j.tet.2011.06.057