(1S,6S)-6-Isopropylamino-3-naphthalen-2-yl-cyclohex-2-enol; hydrochloride

Base Information

Chemical Name:(1S,6S)-6-Isopropylamino-3-naphthalen-2-yl-cyclohex-2-enol; hydrochloride
CAS No.:88141-63-3
Molecular Formula:C₁₉H₂₃NO*ClH
Molecular Weight:317.859
Hs Code.:

Synonyms:(1S,6S)-6-Isopropylamino-3-naphthalen-2-yl-cyclohex-2-enol; hydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1S,6S)-6-Isopropylamino-3-naphthalen-2-yl-cyclohex-2-enol; hydrochloride

Chemical Property:

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Technology Process of (1S,6S)-6-Isopropylamino-3-naphthalen-2-yl-cyclohex-2-enol; hydrochloride

There total 3 articles about (1S,6S)-6-Isopropylamino-3-naphthalen-2-yl-cyclohex-2-enol; hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 88141-54-2
(1S,6S)-6-Amino-3-naphthalen-2-yl-cyclohex-2-enol; hydrochloride

: 67-64-1
acetone

: 88141-63-3
(1S,6S)-6-Isopropylamino-3-naphthalen-2-yl-cyclohex-2-enol; hydrochloride

Guidance literature:: With hydrogenchloride; sodium cyanoborohydride; In methanol; for 72h; Ambient temperature;
DOI:10.1248/cpb.31.2016

Reference yield:

: 88141-46-2
N-(4-Naphthalen-2-yl-2-oxo-cyclohex-3-enyl)-acetamide

: 88141-63-3
(1S,6S)-6-Isopropylamino-3-naphthalen-2-yl-cyclohex-2-enol; hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / NaBH₄ / methanol / 0.17 h / Ambient temperature

2: 81 percent / 1.) 10percent NaOH, 2.) 7N HCl-EtOH / ethanol / 20 h / 70 - 80 °C

3: 87 percent / 1.) NaBH₃CN, 2.) 10percent HCl-EtOH / methanol / 72 h / Ambient temperature

With hydrogenchloride; sodium hydroxide; sodium tetrahydroborate; sodium cyanoborohydride; In methanol; ethanol;
DOI:10.1248/cpb.31.2016

Reference yield:

: 88141-50-8
N-((1S,2S)-2-Hydroxy-4-naphthalen-2-yl-cyclohex-3-enyl)-acetamide

: 88141-63-3
(1S,6S)-6-Isopropylamino-3-naphthalen-2-yl-cyclohex-2-enol; hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / 1.) 10percent NaOH, 2.) 7N HCl-EtOH / ethanol / 20 h / 70 - 80 °C

2: 87 percent / 1.) NaBH₃CN, 2.) 10percent HCl-EtOH / methanol / 72 h / Ambient temperature

With hydrogenchloride; sodium hydroxide; sodium cyanoborohydride; In methanol; ethanol;
DOI:10.1248/cpb.31.2016