3,6-bis(dimethylamino)-9-(methylmercapto)acridine

Base Information

Chemical Name:3,6-bis(dimethylamino)-9-(methylmercapto)acridine
CAS No.:95167-67-2
Molecular Formula:C₁₈H₂₁N₃S
Molecular Weight:311.451
Hs Code.:

Synonyms:3,6-bis(dimethylamino)-9-(methylmercapto)acridine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,6-bis(dimethylamino)-9-(methylmercapto)acridine

Chemical Property:

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Technology Process of 3,6-bis(dimethylamino)-9-(methylmercapto)acridine

There total 2 articles about 3,6-bis(dimethylamino)-9-(methylmercapto)acridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 494-38-2
acridine orange

: 74-88-4
methyl iodide

: 95167-67-2
3,6-bis(dimethylamino)-9-(methylmercapto)acridine

Guidance literature:: With ethanol; sodium ethanolate; Multistep reaction;
DOI:10.1021/jm00036a014

Reference yield:

: 494-38-2
acridine orange

: 95167-67-2
3,6-bis(dimethylamino)-9-(methylmercapto)acridine

Guidance literature:: Multi-step reaction with 2 steps

1: sulfur / neat (no solvent) / 0.5 h / 205 °C

2: sodium / ethanol / 0.5 h / Inert atmosphere; Reflux

With sodium; sulfur; In ethanol;
DOI:10.1080/14756366.2017.1302441

Reference yield: 45.0%

: 95167-67-2
3,6-bis(dimethylamino)-9-(methylmercapto)acridine

: 35303-76-5
4-(2-aminoethyl)benzenesulfonamide

: 4-(2-((3,6-bis(dimethylamino)acridin-9-yl)amino)ethyl)benzenesulfonamide perchlorate

Guidance literature:: 3,6-bis(dimethylamino)-9-(methylmercapto)acridine; 4-(2-aminoethyl)benzenesulfonamide; In N,N-dimethyl acetamide; at 140 ℃; for 2h; Inert atmosphere;

With perchloric acid; In N,N-dimethyl acetamide; water; at 0 ℃; for 1h; Inert atmosphere;
DOI:10.1080/14756366.2017.1302441