2-((1E,3E)-6,6-Dibromo-3-methyl-hexa-1,3,5-trienyl)-1,3,3-trimethyl-cyclohexene

Base Information

Chemical Name:2-((1E,3E)-6,6-Dibromo-3-methyl-hexa-1,3,5-trienyl)-1,3,3-trimethyl-cyclohexene
CAS No.:100846-84-2
Molecular Formula:C₁₆H₂₂Br₂
Molecular Weight:374.159
Hs Code.:

Synonyms:2-((1E,3E)-6,6-Dibromo-3-methyl-hexa-1,3,5-trienyl)-1,3,3-trimethyl-cyclohexene

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Chemical Property of 2-((1E,3E)-6,6-Dibromo-3-methyl-hexa-1,3,5-trienyl)-1,3,3-trimethyl-cyclohexene

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Technology Process of 2-((1E,3E)-6,6-Dibromo-3-methyl-hexa-1,3,5-trienyl)-1,3,3-trimethyl-cyclohexene

There total 2 articles about 2-((1E,3E)-6,6-Dibromo-3-methyl-hexa-1,3,5-trienyl)-1,3,3-trimethyl-cyclohexene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 558-13-4
carbon tetrabromide

: 3917-41-7
(2E,4E)-3-methyl-5-(2,6,6-trimethyl-1-cyclohexen-1-yl)-2,4-pentadienal

: 100846-84-2
2-((1E,3E)-6,6-Dibromo-3-methyl-hexa-1,3,5-trienyl)-1,3,3-trimethyl-cyclohexene

Guidance literature:: With triphenylphosphine;
DOI:10.1016/S0040-4039(00)98860-9

Reference yield:

: 558-13-4
carbon tetrabromide

: 3917-41-7
(2E,4E)-3-methyl-5-(2,6,6-trimethyl-1-cyclohexen-1-yl)-2,4-pentadienal

: 100846-84-2
2-((1E,3E)-6,6-Dibromo-3-methyl-hexa-1,3,5-trienyl)-1,3,3-trimethyl-cyclohexene

: 1-((1E,3Z)-4-Bromo-3-methyl-hexa-1,3,5-trienyl)-2,6,6-trimethyl-cyclohexa-1,3-diene

Guidance literature:: With triphenylphosphine; In dichloromethane; at 0 ℃; for 0.0833333h; Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1002/(SICI)1521-3773(19980216)37:3<320::AID-ANIE320>3.0.CO;2-4

Reference yield: 86.0%

: 100846-84-2
2-((1E,3E)-6,6-Dibromo-3-methyl-hexa-1,3,5-trienyl)-1,3,3-trimethyl-cyclohexene

: 204326-62-5
2-((1E,3E,5Z)-6-Bromo-3-methyl-hexa-1,3,5-trienyl)-1,3,3-trimethyl-cyclohexene

Guidance literature:: With tri-n-butyl-tin hydride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In benzene; for 0.333333h; Ambient temperature;
DOI:10.1002/(SICI)1521-3773(19980216)37:3<320::AID-ANIE320>3.0.CO;2-4