N-[2-(3,4,5-trimethoxyphenyl)-2-phenylethyl]-4-methylbenzenesulphonamide

Base Information

Chemical Name:N-[2-(3,4,5-trimethoxyphenyl)-2-phenylethyl]-4-methylbenzenesulphonamide
CAS No.:1228175-58-3
Molecular Formula:C₂₄H₂₇NO₅S
Molecular Weight:441.548
Hs Code.:

Synonyms:N-[2-(3,4,5-trimethoxyphenyl)-2-phenylethyl]-4-methylbenzenesulphonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[2-(3,4,5-trimethoxyphenyl)-2-phenylethyl]-4-methylbenzenesulphonamide

Chemical Property:

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Technology Process of N-[2-(3,4,5-trimethoxyphenyl)-2-phenylethyl]-4-methylbenzenesulphonamide

There total 1 articles about N-[2-(3,4,5-trimethoxyphenyl)-2-phenylethyl]-4-methylbenzenesulphonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 634-36-6
1,2,3-trimethoxybenzene

: 24395-14-0
N-(p-tolylsulfonyl)-2-phenylaziridine

: 1228175-58-3
N-[2-(3,4,5-trimethoxyphenyl)-2-phenylethyl]-4-methylbenzenesulphonamide

Guidance literature:: With [Ag(COD)2](+)PF₆(-); In 1,2-dichloro-ethane; at 30 - 35 ℃; for 3h; regioselective reaction; Inert atmosphere;
DOI:10.1021/jo100260k

Reference yield:

: 1228175-58-3
N-[2-(3,4,5-trimethoxyphenyl)-2-phenylethyl]-4-methylbenzenesulphonamide

: 104-88-1
4-chlorobenzaldehyde

: 1-(4-chlorophenyl)-5,6,7-trimethoxy-4-phenyl-2-tosyl-1,2,3,4-tetrahydroisoquinoline

: 1-(4-chlorophenyl)-5,6,7-trimethoxy-4-phenyl-2-tosyl-1,2,3,4-tetrahydroisoquinoline

Guidance literature:: With boron trifluoride diethyl etherate; magnesium sulfate; In dichloromethane; at 60 ℃; for 18h; diastereoselective reaction; Inert atmosphere;
DOI:10.1016/j.tet.2015.06.013