13-methyl-2,14-dioxo-17 (2-(pyridin-2-yl)-5-trifluoromethylphenylcarbamoyloxy)-3,13-diazatricyclo[13.3.0.0^4,6]octadec-7-ene-4-carboxylic acid ethyl ester

Base Information

• Chemical Name: 13-methyl-2,14-dioxo-17 (2-(pyridin-2-yl)-5-trifluoromethylphenylcarbamoyloxy)-3,13-diazatricyclo[13.3.0.0^4,6]octadec-7-ene-4-carboxylic acid ethyl ester
• CAS No.: 1045866-35-0
• Molecular Formula: C₃₃H₃₇F₃N₄O₆
• Molecular Weight: 642.675

Synonyms:13-methyl-2,14-dioxo-17 (2-(pyridin-2-yl)-5-trifluoromethylphenylcarbamoyloxy)-3,13-diazatricyclo[13.3.0.0^4,6]octadec-7-ene-4-carboxylic acid ethyl ester

Chemical Property of 13-methyl-2,14-dioxo-17 (2-(pyridin-2-yl)-5-trifluoromethylphenylcarbamoyloxy)-3,13-diazatricyclo[13.3.0.0^4,6]octadec-7-ene-4-carboxylic acid ethyl ester

Chemical Property:

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Technology Process of 13-methyl-2,14-dioxo-17 (2-(pyridin-2-yl)-5-trifluoromethylphenylcarbamoyloxy)-3,13-diazatricyclo[13.3.0.0^4,6]octadec-7-ene-4-carboxylic acid ethyl ester

There total 1 articles about 13-methyl-2,14-dioxo-17 (2-(pyridin-2-yl)-5-trifluoromethylphenylcarbamoyloxy)-3,13-diazatricyclo[13.3.0.0^4,6]octadec-7-ene-4-carboxylic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

phosgene (75-44-5) + 17-hydroxy-13-methyl-2,14-dioxo-3,13-diazatricyclo[13.3.0.04,6]octadec-7-ene-4-carboxylic acid ethyl ester (1045866-34-9) + 2-(pyridin-2-yl)-5-(trifluoromethyl)aniline (158461-46-2) → 13-methyl-2,14-dioxo-17 (2-(pyridin-2-yl)-5-trifluoromethylphenylcarbamoyloxy)-3,13-diazatricyclo[13.3.0.04,6]octadec-7-ene-4-carboxylic acid ethyl ester (1045866-35-0)

Guidance literature:

phosgene; 17-hydroxy-13-methyl-2,14-dioxo-3,13-diazatricyclo[13.3.0.0^4,6]octadec-7-ene-4-carboxylic acid ethyl ester; With sodium hydrogencarbonate; In 1,2-dichloro-ethane; toluene; at 20 ℃; for 2 - 3h;

2-(pyridin-2-yl)-5-(trifluoromethyl)aniline; With 4 A molecular sieve; potassium carbonate; In 1,2-dichloro-ethane; at 100 ℃; for 0.75h; Microwave oven;

Reference yield:

13-methyl-2,14-dioxo-17 (2-(pyridin-2-yl)-5-trifluoromethylphenylcarbamoyloxy)-3,13-diazatricyclo[13.3.0.04,6]octadec-7-ene-4-carboxylic acid ethyl ester (1045866-35-0) → 13-methyl-2,14-dioxo-17 (2-(pyridin-2-yl)-5-trifluoromethylphenylcarbamoyloxy)-3,13-diazatricyclo[13.3.0.04,6]octadec-7-ene-4-carboxylic acid (1045866-36-1)

Guidance literature:

13-methyl-2,14-dioxo-17 (2-(pyridin-2-yl)-5-trifluoromethylphenylcarbamoyloxy)-3,13-diazatricyclo[13.3.0.0^4,6]octadec-7-ene-4-carboxylic acid ethyl ester; With lithium hydroxide; water; In tetrahydrofuran; methanol; at 20 ℃; for 96h;

With 1-hydroxy-1,1,2-ethanetricarboxylic acid; In tetrahydrofuran; methanol; water; pH=~ 4;

upstream raw materials:

phosgene

17-hydroxy-13-methyl-2,14-dioxo-3,13-diazatricyclo[13.3.0.0^4,6]octadec-7-ene-4-carboxylic acid ethyl ester

2-(pyridin-2-yl)-5-(trifluoromethyl)aniline

Downstream raw materials:

13-methyl-2,14-dioxo-17 (2-(pyridin-2-yl)-5-trifluoromethylphenylcarbamoyloxy)-3,13-diazatricyclo[13.3.0.0^4,6]octadec-7-ene-4-carboxylic acid

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