methyl 9-(3-(((3,5-difluorophenyl)sulfonyl)amino)propyl)-2,3,4,9-tetrahydro-1H-carbazole-6-carboxylate

Base Information

Chemical Name:methyl 9-(3-(((3,5-difluorophenyl)sulfonyl)amino)propyl)-2,3,4,9-tetrahydro-1H-carbazole-6-carboxylate
CAS No.:1181975-42-7
Molecular Formula:C₂₃H₂₄F₂N₂O₄S
Molecular Weight:462.517
Hs Code.:

Synonyms:methyl 9-(3-(((3,5-difluorophenyl)sulfonyl)amino)propyl)-2,3,4,9-tetrahydro-1H-carbazole-6-carboxylate

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Chemical Property of methyl 9-(3-(((3,5-difluorophenyl)sulfonyl)amino)propyl)-2,3,4,9-tetrahydro-1H-carbazole-6-carboxylate

Chemical Property:

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Technology Process of methyl 9-(3-(((3,5-difluorophenyl)sulfonyl)amino)propyl)-2,3,4,9-tetrahydro-1H-carbazole-6-carboxylate

There total 8 articles about methyl 9-(3-(((3,5-difluorophenyl)sulfonyl)amino)propyl)-2,3,4,9-tetrahydro-1H-carbazole-6-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 9-(3-aminopropyl)-6,7,8,9-tetrahydro-5H-carbazole-3-carboxylic acid methyl ester trifluoroacetate

: 210532-25-5
3,5-difluorobenzenesulfonyl chloride

: 1181975-42-7
methyl 9-(3-(((3,5-difluorophenyl)sulfonyl)amino)propyl)-2,3,4,9-tetrahydro-1H-carbazole-6-carboxylate

Guidance literature:: 9-(3-aminopropyl)-6,7,8,9-tetrahydro-5H-carbazole-3-carboxylic acid methyl ester trifluoroacetate; With triethylamine; In dichloromethane; at 0 ℃; for 0.0833333h;

3,5-difluorobenzenesulfonyl chloride; In dichloromethane; for 3h;

Reference yield:

: 1181975-72-3
methyl 9-(3-aminopropyl)-2,3,4,9-tetrahydro-1H-carbazole-6-carboxylate

: 210532-25-5
3,5-difluorobenzenesulfonyl chloride

: 1181975-42-7
methyl 9-(3-(((3,5-difluorophenyl)sulfonyl)amino)propyl)-2,3,4,9-tetrahydro-1H-carbazole-6-carboxylate

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃;
DOI:10.1016/j.bmcl.2011.09.019

Reference yield:

: 1181975-01-8
9-(3-tert-butoxycarbonylaminopropyl)-6,7,8,9-tetrahydro-5H-carbazole-3-carboxylic acid methyl ester

: 1181975-42-7
methyl 9-(3-(((3,5-difluorophenyl)sulfonyl)amino)propyl)-2,3,4,9-tetrahydro-1H-carbazole-6-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / dichloromethane / 3 h / 0 - 20 °C

2: triethylamine / dichloromethane / 20 °C

With triethylamine; trifluoroacetic acid; In dichloromethane;
DOI:10.1016/j.bmcl.2011.09.019