O-benzoyl-N-(3-(10,11-dihydro-5H-dibenzo[a,d][7]annulen-5-ylidene)propyl)-N-methylhydroxylamine

Base Information

Chemical Name:O-benzoyl-N-(3-(10,11-dihydro-5H-dibenzo[a,d][7]annulen-5-ylidene)propyl)-N-methylhydroxylamine
CAS No.:5253-86-1
Molecular Formula:C₂₆H₂₅NO₂
Molecular Weight:383.49
Hs Code.:

Synonyms:O-benzoyl-N-(3-(10,11-dihydro-5H-dibenzo[a,d][7]annulen-5-ylidene)propyl)-N-methylhydroxylamine

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Chemical Property of O-benzoyl-N-(3-(10,11-dihydro-5H-dibenzo[a,d][7]annulen-5-ylidene)propyl)-N-methylhydroxylamine

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Technology Process of O-benzoyl-N-(3-(10,11-dihydro-5H-dibenzo[a,d][7]annulen-5-ylidene)propyl)-N-methylhydroxylamine

There total 5 articles about O-benzoyl-N-(3-(10,11-dihydro-5H-dibenzo[a,d][7]annulen-5-ylidene)propyl)-N-methylhydroxylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5253-85-0
N-[3-(10,11-Dihydro-dibenzo[a,d]cyclohepten-5-ylidene)-propyl]-N-methyl-hydroxylamine

: 98-88-4
benzoyl chloride

: 5253-86-1
O-benzoyl-N-(3-(10,11-dihydro-5H-dibenzo[a,d][7]annulen-5-ylidene)propyl)-N-methylhydroxylamine

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 0 ℃; Inert atmosphere;
DOI:10.1021/acs.orglett.8b03787

Reference yield:

: 894-71-3
nortriptyline hydrochloride

: 5253-86-1
O-benzoyl-N-(3-(10,11-dihydro-5H-dibenzo[a,d][7]annulen-5-ylidene)propyl)-N-methylhydroxylamine

Guidance literature:: Multi-step reaction with 4 steps

1: sodium / methanol / 12 h / 55 °C / Inert atmosphere

2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / -78 °C / Inert atmosphere

3: dichloromethane / 25 °C / Inert atmosphere

4: triethylamine; dmap / dichloromethane / 0 °C / Inert atmosphere

With dmap; sodium; triethylamine; 3-chloro-benzenecarboperoxoic acid; In methanol; dichloromethane; 3: |Cope Elimination;
DOI:10.1021/acs.orglett.8b03787

Reference yield:

: 3-((3-(10,11-dihydro-5H-dibenzo[a,d][7]annulen-5-ylidene)propyl)(methyl)amino)propanenitrile

: 5253-86-1
O-benzoyl-N-(3-(10,11-dihydro-5H-dibenzo[a,d][7]annulen-5-ylidene)propyl)-N-methylhydroxylamine

Guidance literature:: Multi-step reaction with 3 steps

1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / -78 °C / Inert atmosphere

2: dichloromethane / 25 °C / Inert atmosphere

3: triethylamine; dmap / dichloromethane / 0 °C / Inert atmosphere

With dmap; triethylamine; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; 2: |Cope Elimination;
DOI:10.1021/acs.orglett.8b03787