N-(2-(3-(6-methyl-2-oxo-1,2-dihydropyridin-4-yl)phenoxy)ethyl)-2-nitrobenzenesulfonamide

Base Information

Chemical Name:N-(2-(3-(6-methyl-2-oxo-1,2-dihydropyridin-4-yl)phenoxy)ethyl)-2-nitrobenzenesulfonamide
CAS No.:1416332-51-8
Molecular Formula:C₂₀H₁₉N₃O₆S
Molecular Weight:429.453
Hs Code.:

Synonyms:N-(2-(3-(6-methyl-2-oxo-1,2-dihydropyridin-4-yl)phenoxy)ethyl)-2-nitrobenzenesulfonamide

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Chemical Property of N-(2-(3-(6-methyl-2-oxo-1,2-dihydropyridin-4-yl)phenoxy)ethyl)-2-nitrobenzenesulfonamide

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Technology Process of N-(2-(3-(6-methyl-2-oxo-1,2-dihydropyridin-4-yl)phenoxy)ethyl)-2-nitrobenzenesulfonamide

There total 7 articles about N-(2-(3-(6-methyl-2-oxo-1,2-dihydropyridin-4-yl)phenoxy)ethyl)-2-nitrobenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.1%

: 1416332-44-9
(E)-2-nitro-N-(2-(3-(3-oxobut-1-en-1-yl)phenoxy)ethyl)benzenesulfonamide

: 49639-34-1,90617-28-0
phenylsulfinylacetic acid amide

: 1416332-51-8
N-(2-(3-(6-methyl-2-oxo-1,2-dihydropyridin-4-yl)phenoxy)ethyl)-2-nitrobenzenesulfonamide

Guidance literature:: (E)-2-nitro-N-(2-(3-(3-oxobut-1-en-1-yl)phenoxy)ethyl)benzenesulfonamide; phenylsulfinylacetic acid amide; With 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium chloride; In acetonitrile; at 50 ℃; for 4h; Inert atmosphere;

With acetic acid; In acetonitrile; for 3h; Inert atmosphere; Reflux;
DOI:10.1021/ol500162b

Reference yield:

: C₂₃H₂₆N₂O₈S

: 1416332-51-8
N-(2-(3-(6-methyl-2-oxo-1,2-dihydropyridin-4-yl)phenoxy)ethyl)-2-nitrobenzenesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1: trifluoroacetic acid / dichloromethane / 5 h / 20 °C / Inert atmosphere

2: 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium chloride / acetonitrile / 4 h / 50 °C / Inert atmosphere

3: acetic acid / acetonitrile / Inert atmosphere; Reflux

4: acetic acid / acetonitrile / Inert atmosphere; Reflux

With acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; trifluoroacetic acid; lithium chloride; In dichloromethane; acetonitrile;
DOI:10.1021/ol303320c

Reference yield:

: 1416332-44-9
(E)-2-nitro-N-(2-(3-(3-oxobut-1-en-1-yl)phenoxy)ethyl)benzenesulfonamide

: 1416332-51-8
N-(2-(3-(6-methyl-2-oxo-1,2-dihydropyridin-4-yl)phenoxy)ethyl)-2-nitrobenzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium chloride / acetonitrile / 4 h / 50 °C / Inert atmosphere

2: acetic acid / acetonitrile / Inert atmosphere; Reflux

3: acetic acid / acetonitrile / Inert atmosphere; Reflux

With acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium chloride; In acetonitrile;
DOI:10.1021/ol303320c