(E)-2-nitro-N-(2-(3-(3-oxobut-1-en-1-yl)phenoxy)ethyl)benzenesulfonamide

Base Information

Chemical Name:(E)-2-nitro-N-(2-(3-(3-oxobut-1-en-1-yl)phenoxy)ethyl)benzenesulfonamide
CAS No.:1416332-44-9
Molecular Formula:C₁₈H₁₈N₂O₆S
Molecular Weight:390.417
Hs Code.:

Synonyms:(E)-2-nitro-N-(2-(3-(3-oxobut-1-en-1-yl)phenoxy)ethyl)benzenesulfonamide

Suppliers and Price of (E)-2-nitro-N-(2-(3-(3-oxobut-1-en-1-yl)phenoxy)ethyl)benzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-2-nitro-N-(2-(3-(3-oxobut-1-en-1-yl)phenoxy)ethyl)benzenesulfonamide

Chemical Property:

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Technology Process of (E)-2-nitro-N-(2-(3-(3-oxobut-1-en-1-yl)phenoxy)ethyl)benzenesulfonamide

There total 3 articles about (E)-2-nitro-N-(2-(3-(3-oxobut-1-en-1-yl)phenoxy)ethyl)benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₃H₂₆N₂O₈S

: 1416332-44-9
(E)-2-nitro-N-(2-(3-(3-oxobut-1-en-1-yl)phenoxy)ethyl)benzenesulfonamide

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 5h; Inert atmosphere;
DOI:10.1021/ol303320c DOI:10.1021/ol500162b

Reference yield:

: 1416332-52-9
(E)-4-(3-(2-hydroxyethoxy)phenyl)but-3-en-2-one

: 1416332-44-9
(E)-2-nitro-N-(2-(3-(3-oxobut-1-en-1-yl)phenoxy)ethyl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: triphenylphosphine; diethylazodicarboxylate / benzene; toluene / 0 - 20 °C / Inert atmosphere

2: trifluoroacetic acid / dichloromethane / 5 h / 20 °C / Inert atmosphere

With triphenylphosphine; trifluoroacetic acid; diethylazodicarboxylate; In dichloromethane; toluene; benzene;
DOI:10.1021/ol500162b

Reference yield:

: 20511-03-9,22214-29-5
4-(3’-hydroxyphenyl)-3(E)-buten-2-one

: 1416332-44-9
(E)-2-nitro-N-(2-(3-(3-oxobut-1-en-1-yl)phenoxy)ethyl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: tetra-(n-butyl)ammonium iodide; potassium carbonate / dimethyl sulfoxide / 5 h / 100 °C / Inert atmosphere

2: triphenylphosphine; diethylazodicarboxylate / benzene; toluene / 0 - 20 °C / Inert atmosphere

3: trifluoroacetic acid / dichloromethane / 5 h / 20 °C / Inert atmosphere

With tetra-(n-butyl)ammonium iodide; potassium carbonate; triphenylphosphine; trifluoroacetic acid; diethylazodicarboxylate; In dichloromethane; dimethyl sulfoxide; toluene; benzene;
DOI:10.1021/ol500162b