5-(2,4-bisbenzyloxy-5-bromophenyl)-4-(2-methylphenyl)-3-hydroxy-4H-1,2,4-triazole

Base Information

Chemical Name:5-(2,4-bisbenzyloxy-5-bromophenyl)-4-(2-methylphenyl)-3-hydroxy-4H-1,2,4-triazole
CAS No.:958253-50-4
Molecular Formula:C₂₉H₂₄BrN₃O₃
Molecular Weight:542.432
Hs Code.:

Synonyms:5-(2,4-bisbenzyloxy-5-bromophenyl)-4-(2-methylphenyl)-3-hydroxy-4H-1,2,4-triazole

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Chemical Property of 5-(2,4-bisbenzyloxy-5-bromophenyl)-4-(2-methylphenyl)-3-hydroxy-4H-1,2,4-triazole

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Technology Process of 5-(2,4-bisbenzyloxy-5-bromophenyl)-4-(2-methylphenyl)-3-hydroxy-4H-1,2,4-triazole

There total 1 articles about 5-(2,4-bisbenzyloxy-5-bromophenyl)-4-(2-methylphenyl)-3-hydroxy-4H-1,2,4-triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1005175-45-0
N-(2-methylphenyl)-3-bromo-4,6-dibenzyloxybenzamide hydrazone

: 530-62-1
1,1'-carbonyldiimidazole

: 958253-50-4
5-(2,4-bisbenzyloxy-5-bromophenyl)-4-(2-methylphenyl)-3-hydroxy-4H-1,2,4-triazole

Guidance literature:: In tetrahydrofuran; at 3 - 25 ℃;

Reference yield: 70.0%

: 110-68-9
N-n-butyl-N-methylamine

: 201230-82-2
carbon monoxide

: 958253-50-4
5-(2,4-bisbenzyloxy-5-bromophenyl)-4-(2-methylphenyl)-3-hydroxy-4H-1,2,4-triazole

: 1041201-90-4
5-[4-(2-methylphenyl)-3-hydroxy-4H-1,2,4-triazol-5-yl]-2,4-bisbenzyloxy-N-methyl-N-butylbenzamide

Guidance literature:: With triethylamine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In tetrahydrofuran; at 120 ℃; for 20h; under 3750.38 - 7500.75 Torr; autoclave;

Reference yield:

: 201230-82-2
carbon monoxide

: 958253-50-4
5-(2,4-bisbenzyloxy-5-bromophenyl)-4-(2-methylphenyl)-3-hydroxy-4H-1,2,4-triazole

: 103-67-3
benzyl-methyl-amine

: 958251-18-8
5-[2,4-dihydroxy-5-(N-benzyl-N-methylaminocarbonyl)phenyl]-4-(2-methylphenyl)-3-hydroxy-4H-1,2,4-triazole

Guidance literature:: carbon monoxide; 5-(2,4-bisbenzyloxy-5-bromophenyl)-4-(2-methylphenyl)-3-hydroxy-4H-1,2,4-triazole; With triethylamine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In methanol; toluene; at 100 ℃; for 5h; under 3000.3 - 6000.6 Torr;

With sodium hydroxide; In tetrahydrofuran; methanol;

benzyl-methyl-amine;