N-[(3,5-diisopropoxy)phenyl] 4-[(2-amino)ethoxy]-3,5-dimethylbenzamide hydrochloride

Base Information

Chemical Name:N-[(3,5-diisopropoxy)phenyl] 4-[(2-amino)ethoxy]-3,5-dimethylbenzamide hydrochloride
CAS No.:1032435-05-4
Molecular Formula:C₂₃H₃₂N₂O₄*ClH
Molecular Weight:436.979
Hs Code.:

Synonyms:N-[(3,5-diisopropoxy)phenyl] 4-[(2-amino)ethoxy]-3,5-dimethylbenzamide hydrochloride

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Chemical Property of N-[(3,5-diisopropoxy)phenyl] 4-[(2-amino)ethoxy]-3,5-dimethylbenzamide hydrochloride

Chemical Property:

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Technology Process of N-[(3,5-diisopropoxy)phenyl] 4-[(2-amino)ethoxy]-3,5-dimethylbenzamide hydrochloride

There total 10 articles about N-[(3,5-diisopropoxy)phenyl] 4-[(2-amino)ethoxy]-3,5-dimethylbenzamide hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1006584-05-9
C₂₈H₄₀N₂O₆

: 1032435-05-4
N-[(3,5-diisopropoxy)phenyl] 4-[(2-amino)ethoxy]-3,5-dimethylbenzamide hydrochloride

Guidance literature:: With hydrogenchloride; In diethyl ether; at 20 ℃;
DOI:10.1021/jm701359z

Reference yield:

: 150242-82-3
3,5-di-(isopropyloxy)benzoic acid

: 1032435-05-4
N-[(3,5-diisopropoxy)phenyl] 4-[(2-amino)ethoxy]-3,5-dimethylbenzamide hydrochloride

Guidance literature:: Multi-step reaction with 5 steps

1: diphenylphosphoranyl azide; triethylamine / toluene / 2 h / 20 °C

2: toluene / 16 h / Heating

3: hydrogenchloride / 1,4-dioxane / 3 h / 20 °C

4: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / N,N-dimethyl-formamide / 16 h

5: hydrogenchloride / diethyl ether / 20 °C

With hydrogenchloride; diphenylphosphoranyl azide; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In 1,4-dioxane; diethyl ether; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jm701359z

Reference yield:

: 942998-95-0
methyl 4-[2-(tert-butyloxycarbonylamino)ethoxy]-3,5-dimethylbenzoate

: 1032435-05-4
N-[(3,5-diisopropoxy)phenyl] 4-[(2-amino)ethoxy]-3,5-dimethylbenzamide hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: potassium hydroxide / methanol / 3 h / 50 °C

2: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / N,N-dimethyl-formamide / 16 h

3: hydrogenchloride / diethyl ether / 20 °C

With hydrogenchloride; potassium hydroxide; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In methanol; diethyl ether; N,N-dimethyl-formamide;
DOI:10.1021/jm701359z