ethyl <3-(3',4'-dichlorobenzyl)-1,2,3,4-tetrahydro-2,4-dioxoquinazolin-1-yl> acetate

Base Information

Chemical Name:ethyl <3-(3',4'-dichlorobenzyl)-1,2,3,4-tetrahydro-2,4-dioxoquinazolin-1-yl> acetate
CAS No.:112733-05-8
Molecular Formula:C₁₉H₁₆Cl₂N₂O₄
Molecular Weight:407.253
Hs Code.:

Synonyms:ethyl <3-(3',4'-dichlorobenzyl)-1,2,3,4-tetrahydro-2,4-dioxoquinazolin-1-yl> acetate

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Chemical Property of ethyl <3-(3',4'-dichlorobenzyl)-1,2,3,4-tetrahydro-2,4-dioxoquinazolin-1-yl> acetate

Chemical Property:

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Technology Process of ethyl <3-(3',4'-dichlorobenzyl)-1,2,3,4-tetrahydro-2,4-dioxoquinazolin-1-yl> acetate

There total 4 articles about ethyl <3-(3',4'-dichlorobenzyl)-1,2,3,4-tetrahydro-2,4-dioxoquinazolin-1-yl> acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 112733-60-5
3-(3',4'-dichlorobenzyl)-1,2,3,4-tetrahydro-2,4-dioxoquinazoline

: 105-36-2
ethyl bromoacetate

: 112733-05-8
ethyl <3-(3',4'-dichlorobenzyl)-1,2,3,4-tetrahydro-2,4-dioxoquinazolin-1-yl> acetate

Guidance literature:: With sodium hydride; Yield given. Multistep reaction; 1.) DMF, 50 deg C, 1 h, 2.) 90 deg C, 7 h;
DOI:10.1016/0223-5234(90)90019-Y

Reference yield:

: 118-48-9
isatoic anhydride

: 112733-05-8
ethyl <3-(3',4'-dichlorobenzyl)-1,2,3,4-tetrahydro-2,4-dioxoquinazolin-1-yl> acetate

Guidance literature:: Multi-step reaction with 3 steps

1: 77 percent / ethanol / 2 h / Heating

2: N-methyl pyrrolidinone / 12 h / 180 °C

3: 1.) sodium hydride / 1.) DMF, 50 deg C, 1 h, 2.) 90 deg C, 7 h

With 1-methyl-pyrrolidin-2-one; sodium hydride; In ethanol;
DOI:10.1016/0223-5234(90)90019-Y

Reference yield:

: 102-49-8
3,4-dichlorobenzyl amine

: 112733-05-8
ethyl <3-(3',4'-dichlorobenzyl)-1,2,3,4-tetrahydro-2,4-dioxoquinazolin-1-yl> acetate

Guidance literature:: Multi-step reaction with 3 steps

1: 77 percent / ethanol / 2 h / Heating

2: N-methyl pyrrolidinone / 12 h / 180 °C

3: 1.) sodium hydride / 1.) DMF, 50 deg C, 1 h, 2.) 90 deg C, 7 h

With 1-methyl-pyrrolidin-2-one; sodium hydride; In ethanol;
DOI:10.1016/0223-5234(90)90019-Y