C₃₉H₃₉N₄O₁₃P₂S₄^(1-)

Base Information

Chemical Name:C₃₉H₃₉N₄O₁₃P₂S₄^(1-)
CAS No.:84774-91-4
Molecular Formula:C₃₉H₃₉N₄O₁₃P₂S₄
Molecular Weight:961.969
Hs Code.:

C<sub>39</sub>H<sub>39</sub>N<sub>4</sub>O<sub>13</sub>P<sub>2</sub>S<sub>4</sub><sup>(1-)</sup>

Synonyms:C₃₉H₃₉N₄O₁₃P₂S₄^(1-)

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Chemical Property of C₃₉H₃₉N₄O₁₃P₂S₄^(1-)

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Technology Process of C₃₉H₃₉N₄O₁₃P₂S₄^(1-)

There total 9 articles about C₃₉H₃₉N₄O₁₃P₂S₄^(1-) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67941-87-1
cyclohexylammonium S,S-diphenyl phosphorodithioate

: 84774-91-4
C₃₉H₃₉N₄O₁₃P₂S₄^(1-)

Guidance literature:: Multi-step reaction with 4 steps

1: 87 percent / mesitylene 1,3-disulfonyl chloride / pyridine / 5 h

2: pyridinium phosphinate, TEA / pyridine / 0.25 h / Ambient temperature

3: mesitylene 1,3-disulfonyl chloride, 3-nitro-1,2,4-triazole / pyridine / 0.67 h / Ambient temperature

4: pyridinium phosphinate, TEA / pyridine / 0.25 h / Ambient temperature

With H₂O₂P*C₅H₅N; TEA; 2,4,6-trimethyl-1,3-benzenedisulfonyl dichloride; 3-nitro-1,2,4-triazole; In pyridine;
DOI:10.1021/ja00345a062

Reference yield:

: 21090-30-2
3'-O-acetylthymidine

: 84774-91-4
C₃₉H₃₉N₄O₁₃P₂S₄^(1-)

Guidance literature:: Multi-step reaction with 6 steps

1: 53 percent / TsOH*H₂O, molecular sieves / dioxane / 1 h

2: 96 percent / BuNH₂ / methanol / 3 h / Ambient temperature

3: 87 percent / mesitylene 1,3-disulfonyl chloride / pyridine / 5 h

4: pyridinium phosphinate, TEA / pyridine / 0.25 h / Ambient temperature

5: mesitylene 1,3-disulfonyl chloride, 3-nitro-1,2,4-triazole / pyridine / 0.67 h / Ambient temperature

6: pyridinium phosphinate, TEA / pyridine / 0.25 h / Ambient temperature

With molecular sieve; H₂O₂P*C₅H₅N; TEA; 2,4,6-trimethyl-1,3-benzenedisulfonyl dichloride; toluene-4-sulfonic acid; N-butylamine; 3-nitro-1,2,4-triazole; In 1,4-dioxane; pyridine; methanol;
DOI:10.1021/ja00345a062

Reference yield:

: 84752-63-6
5'-O-(1,3-benzodithiol-2-yl)thymidine

: 84774-91-4
C₃₉H₃₉N₄O₁₃P₂S₄^(1-)

Guidance literature:: Multi-step reaction with 4 steps

1: 87 percent / mesitylene 1,3-disulfonyl chloride / pyridine / 5 h

2: pyridinium phosphinate, TEA / pyridine / 0.25 h / Ambient temperature

3: mesitylene 1,3-disulfonyl chloride, 3-nitro-1,2,4-triazole / pyridine / 0.67 h / Ambient temperature

4: pyridinium phosphinate, TEA / pyridine / 0.25 h / Ambient temperature

With H₂O₂P*C₅H₅N; TEA; 2,4,6-trimethyl-1,3-benzenedisulfonyl dichloride; 3-nitro-1,2,4-triazole; In pyridine;
DOI:10.1021/ja00345a062