(S)-15-Methyl-3-(13-methyl-tetradecanoyloxy)-hexadecanoic acid benzhydryl ester

Base Information

Chemical Name:(S)-15-Methyl-3-(13-methyl-tetradecanoyloxy)-hexadecanoic acid benzhydryl ester
CAS No.:179869-86-4
Molecular Formula:C₄₅H₇₂O₄
Molecular Weight:677.064
Hs Code.:

Synonyms:(S)-15-Methyl-3-(13-methyl-tetradecanoyloxy)-hexadecanoic acid benzhydryl ester

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Chemical Property of (S)-15-Methyl-3-(13-methyl-tetradecanoyloxy)-hexadecanoic acid benzhydryl ester

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Technology Process of (S)-15-Methyl-3-(13-methyl-tetradecanoyloxy)-hexadecanoic acid benzhydryl ester

There total 5 articles about (S)-15-Methyl-3-(13-methyl-tetradecanoyloxy)-hexadecanoic acid benzhydryl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 2485-71-4
13-methyltetradecanoic acid

: 178860-76-9
(S)-3-Hydroxy-15-methyl-hexadecanoic acid benzhydryl ester

: 179869-86-4
(S)-15-Methyl-3-(13-methyl-tetradecanoyloxy)-hexadecanoic acid benzhydryl ester

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; for 16h; Ambient temperature;
DOI:10.1016/S0040-4020(98)83044-5

Reference yield:

: 178860-74-7
(2S,4R)-2,4-((S)-benzylidenedioxy)-1-benzyloxy-16-methylheptadec-5(E/Z)-ene

: 179869-86-4
(S)-15-Methyl-3-(13-methyl-tetradecanoyloxy)-hexadecanoic acid benzhydryl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) H₂, 2.) H₂ / 1.) Pd/C, 2.) Pd(OH)2/C / 1.) THF, from 20 to 25 deg C, 1 h, 2.) MeOH, room temperature, 1 h.

2: 28 mg / NaIO₄ / dioxane; H₂O / 1 h / 24 °C

3: m-chloroperoxybenzoic acid / CHCl₃ / 1 h / 50 °C

4: ethyl acetate / 0.75 h / 50 °C

5: 90 percent / DCC, DMAP / CH₂Cl₂ / 16 h / Ambient temperature

With dmap; sodium periodate; hydrogen; 3-chloro-benzenecarboperoxoic acid; dicyclohexyl-carbodiimide; palladium dihydroxide; palladium on activated charcoal; In 1,4-dioxane; dichloromethane; chloroform; water; ethyl acetate;
DOI:10.1016/S0040-4020(98)83044-5

Reference yield:

: 179869-85-3
(2S,4S)-16-methyl-1,2,4-trihydroxyheptadecane

: 179869-86-4
(S)-15-Methyl-3-(13-methyl-tetradecanoyloxy)-hexadecanoic acid benzhydryl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 28 mg / NaIO₄ / dioxane; H₂O / 1 h / 24 °C

2: m-chloroperoxybenzoic acid / CHCl₃ / 1 h / 50 °C

3: ethyl acetate / 0.75 h / 50 °C

4: 90 percent / DCC, DMAP / CH₂Cl₂ / 16 h / Ambient temperature

With dmap; sodium periodate; 3-chloro-benzenecarboperoxoic acid; dicyclohexyl-carbodiimide; In 1,4-dioxane; dichloromethane; chloroform; water; ethyl acetate;
DOI:10.1016/S0040-4020(98)83044-5