N-[(3S)-15-methyl-3-(13-methyltetradecanoyloxy)hexadecanoyl]glycine benzyl ester

Base Information

Chemical Name:N-[(3S)-15-methyl-3-(13-methyltetradecanoyloxy)hexadecanoyl]glycine benzyl ester
CAS No.:214406-38-9
Molecular Formula:C₄₁H₇₁NO₅
Molecular Weight:658.018
Hs Code.:

Synonyms:

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Chemical Property of N-[(3S)-15-methyl-3-(13-methyltetradecanoyloxy)hexadecanoyl]glycine benzyl ester

Chemical Property:

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Technology Process of N-[(3S)-15-methyl-3-(13-methyltetradecanoyloxy)hexadecanoyl]glycine benzyl ester

There total 9 articles about N-[(3S)-15-methyl-3-(13-methyltetradecanoyloxy)hexadecanoyl]glycine benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2462-31-9
benzyl 2-aminoacetate hydrochloride

: 13-Methyl-tetradecanoic acid (S)-1-chlorocarbonylmethyl-13-methyl-tetradecyl ester

: 214406-38-9
N-[(3S)-15-methyl-3-(13-methyltetradecanoyloxy)hexadecanoyl]glycine benzyl ester

Guidance literature:: With triethylamine; In dichloromethane; at 24 ℃; for 1h; Yield given;
DOI:10.1016/S0040-4039(98)00798-9

Reference yield:

: 2485-71-4
13-methyltetradecanoic acid

: 214406-38-9
N-[(3S)-15-methyl-3-(13-methyltetradecanoyloxy)hexadecanoyl]glycine benzyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / DCC, DMAP / CH₂Cl₂ / 16 h / Ambient temperature

2: 91 percent / H₂ / Pd(OH)2/C / ethanol / 2 h / Ambient temperature

3: oxalyl chloride / CH₂Cl₂ / 1 h / Ambient temperature

4: Et₃N / CH₂Cl₂ / 1 h / 0 - 5 °C

With dmap; oxalyl dichloride; hydrogen; triethylamine; dicyclohexyl-carbodiimide; palladium dihydroxide; In ethanol; dichloromethane;
DOI:10.1016/S0040-4020(98)83044-5

Reference yield:

: 179869-85-3
(2S,4S)-16-methyl-1,2,4-trihydroxyheptadecane

: 214406-38-9
N-[(3S)-15-methyl-3-(13-methyltetradecanoyloxy)hexadecanoyl]glycine benzyl ester

Guidance literature:: Multi-step reaction with 7 steps

1: 28 mg / NaIO₄ / dioxane; H₂O / 1 h / 24 °C

2: m-chloroperoxybenzoic acid / CHCl₃ / 1 h / 50 °C

3: ethyl acetate / 0.75 h / 50 °C

4: 90 percent / DCC, DMAP / CH₂Cl₂ / 16 h / Ambient temperature

5: 91 percent / H₂ / Pd(OH)2/C / ethanol / 2 h / Ambient temperature

6: oxalyl chloride / CH₂Cl₂ / 1 h / Ambient temperature

7: Et₃N / CH₂Cl₂ / 1 h / 0 - 5 °C

With dmap; sodium periodate; oxalyl dichloride; hydrogen; triethylamine; 3-chloro-benzenecarboperoxoic acid; dicyclohexyl-carbodiimide; palladium dihydroxide; In 1,4-dioxane; ethanol; dichloromethane; chloroform; water; ethyl acetate;
DOI:10.1016/S0040-4020(98)83044-5