N⁶-benzoyl-9-[6,7-dideoxy-2,3-O-isopropylidene-β-D-allo-hept-6-ynofuranosyl]adenine

Base Information

• Chemical Name: N⁶-benzoyl-9-[6,7-dideoxy-2,3-O-isopropylidene-β-D-allo-hept-6-ynofuranosyl]adenine
• CAS No.: 244263-92-1
• Molecular Formula: C₂₂H₂₁N₅O₅
• Molecular Weight: 435.439

Synonyms:N⁶-benzoyl-9-[6,7-dideoxy-2,3-O-isopropylidene-β-D-allo-hept-6-ynofuranosyl]adenine

Chemical Property of N⁶-benzoyl-9-[6,7-dideoxy-2,3-O-isopropylidene-β-D-allo-hept-6-ynofuranosyl]adenine

Chemical Property:

Purity/Quality:

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Technology Process of N⁶-benzoyl-9-[6,7-dideoxy-2,3-O-isopropylidene-β-D-allo-hept-6-ynofuranosyl]adenine

There total 1 articles about N⁶-benzoyl-9-[6,7-dideoxy-2,3-O-isopropylidene-β-D-allo-hept-6-ynofuranosyl]adenine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

N6-benzoyl-9-[6,7-dideoxy-2,3-O-isopropylidene-7-C-(trimethylsilyl)-β-D-allo-hept-6-ynofuranosyl]adenine (244263-89-6) → N6-benzoyl-9-[6,7-dideoxy-2,3-O-isopropylidene-β-D-allo-hept-6-ynofuranosyl]adenine (244263-92-1)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; acetic acid; for 0.75h;

DOI:10.1002/hlca.200490269

Reference yield: 90.0%

triethylsilyl chloride (994-30-9) + N6-benzoyl-9-[6,7-dideoxy-2,3-O-isopropylidene-β-D-allo-hept-6-ynofuranosyl]adenine (244263-92-1) → N6-benzoyl-9-[6,7-dideoxy-2,3-O-isopropylidene-5-O-(triethylsilyl)-β-D-allo-hept-6-ynofuranosyl]adenine (323203-87-8)

Guidance literature:

With 1H-imidazole; In N,N-dimethyl-formamide; at 25 ℃; for 12h;

DOI:10.1002/1522-2675(20001108)83:11<2975::AID-HLCA2975>3.0.CO;2-2

Reference yield: 88.0%

triisopropylsilyl trifluoromethanesulfonate (80522-42-5) + N6-benzoyl-9-[6,7-dideoxy-2,3-O-isopropylidene-β-D-allo-hept-6-ynofuranosyl]adenine (244263-92-1) → N6-benzoyl-9-[6,7-dideoxy-2,3-O-isopropylidene-5-O-(triisopropylsilyl)-β-D-allo-hept-6-ynofuranosyl]adenine (847205-26-9)

Guidance literature:

In pyridine; dichloromethane; at 23 ℃; for 1h;

DOI:10.1002/hlca.200490269

upstream raw materials:

N⁶-benzoyl-9-[6,7-dideoxy-2,3-O-isopropylidene-7-C-(trimethylsilyl)-β-D-allo-hept-6-ynofuranosyl]adenine

Downstream raw materials:

N⁶-benzoyl-9-[6,7-dideoxy-2,3-O-isopropylidene-5-O-(triethylsilyl)-β-D-allo-hept-6-ynofuranosyl]adenine

N⁶-benzoyl-9-[6,7-dideoxy-2,3-O-isopropylidene-5-O-(triisopropylsilyl)-β-D-allo-hept-6-ynofuranosyl]adenine

N⁶-benzoyl-2',3'-O-isopropylidene-5'-O-(triethylsilyl)adenosin-8-yl-(8->7'-C)-N⁶-benzoyl-9-[6,7-dideoxy-2,3-O-isopropylidene-β-D-allo-hept-6-ynofuranosyl]adenine

C₆₅H₈₈N₁₀O₁₀Si₃

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