1-[3,5-bis(hydroxymethyl)benzyl]-4-(pyridin-4-yl)pyridinium hexafluorophosphate

Base Information

Chemical Name:1-[3,5-bis(hydroxymethyl)benzyl]-4-(pyridin-4-yl)pyridinium hexafluorophosphate
CAS No.:1220072-33-2
Molecular Formula:C₁₉H₁₉N₂O₂*F₆P
Molecular Weight:452.336
Hs Code.:

Synonyms:1-[3,5-bis(hydroxymethyl)benzyl]-4-(pyridin-4-yl)pyridinium hexafluorophosphate

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Chemical Property of 1-[3,5-bis(hydroxymethyl)benzyl]-4-(pyridin-4-yl)pyridinium hexafluorophosphate

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Technology Process of 1-[3,5-bis(hydroxymethyl)benzyl]-4-(pyridin-4-yl)pyridinium hexafluorophosphate

There total 3 articles about 1-[3,5-bis(hydroxymethyl)benzyl]-4-(pyridin-4-yl)pyridinium hexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1241581-76-9
N-(3,5-di(hydroxymethyl)-benzyl)-4,4’-bipyridinium bromide salt

: 1220072-33-2
1-[3,5-bis(hydroxymethyl)benzyl]-4-(pyridin-4-yl)pyridinium hexafluorophosphate

Guidance literature:: With ammonium hexafluorophosphate; In water;
DOI:10.1021/jm301337y

Reference yield: 91.0%

: 553-26-4
4,4'-bipyridine

: (5-(bromomethyl)-1,3-phenylene)dimethanol

: 1220072-33-2
1-[3,5-bis(hydroxymethyl)benzyl]-4-(pyridin-4-yl)pyridinium hexafluorophosphate

Guidance literature:: 4,4'-bipyridine; (5-(bromomethyl)-1,3-phenylene)dimethanol; In acetonitrile; at 80 ℃; for 16h;

With ammonium hexafluorophosphate; In water; at 50 ℃;
DOI:10.1016/j.tetlet.2010.02.097

Reference yield:

: 4464-18-0
1,3,5-tris(hydroxymethyl)benzene

: 1220072-33-2
1-[3,5-bis(hydroxymethyl)benzyl]-4-(pyridin-4-yl)pyridinium hexafluorophosphate

Guidance literature:: Multi-step reaction with 3 steps

1: triphenylphosphine; carbon tetrabromide / tetrahydrofuran / 2.5 h / 20 °C

2: tetrahydrofuran / 24 h / Reflux

3: ammonium hexafluorophosphate / water

With ammonium hexafluorophosphate; carbon tetrabromide; triphenylphosphine; In tetrahydrofuran; water;
DOI:10.1021/jm301337y