2,5-bis(dodecyloxy)-4-(2'-trimethylsilylethynyl)triisopropylsilylacetylenylbenzene

Base Information

• Chemical Name: 2,5-bis(dodecyloxy)-4-(2'-trimethylsilylethynyl)triisopropylsilylacetylenylbenzene
• CAS No.: 935529-60-5
• Molecular Formula: C₄₆H₈₂O₂Si₂
• Molecular Weight: 723.327

Synonyms:2,5-bis(dodecyloxy)-4-(2'-trimethylsilylethynyl)triisopropylsilylacetylenylbenzene

Chemical Property of 2,5-bis(dodecyloxy)-4-(2'-trimethylsilylethynyl)triisopropylsilylacetylenylbenzene

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

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Technology Process of 2,5-bis(dodecyloxy)-4-(2'-trimethylsilylethynyl)triisopropylsilylacetylenylbenzene

There total 1 articles about 2,5-bis(dodecyloxy)-4-(2'-trimethylsilylethynyl)triisopropylsilylacetylenylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

tris-iso-propylsilyl acetylene (89343-06-6) + 1,4-bis(dodecyloxy)-2-[(trimethylsilyl)ethynyl]-5-iodobenzene (523978-90-7) → 2,5-bis(dodecyloxy)-4-(2'-trimethylsilylethynyl)triisopropylsilylacetylenylbenzene (935529-60-5)

Guidance literature:

With copper diacetate; triphenylphosphine; palladium dichloride; In tetrahydrofuran; triethylamine; at 50 ℃; for 15h;

DOI:10.1039/b810856k

Reference yield: 100.0%

2,5-bis(dodecyloxy)-4-(2'-trimethylsilylethynyl)triisopropylsilylacetylenylbenzene (935529-60-5) → 2,5-bis(dodecyloxy)-4-(2'-ethynyl)triisopropylsilylacetylenylbenzene (1138324-68-1)

Guidance literature:

With potassium carbonate; In methanol; dichloromethane; at 20 ℃; for 3h;

DOI:10.1039/b810856k

upstream raw materials:

tris-iso-propylsilyl acetylene

1,4-bis(dodecyloxy)-2-[(trimethylsilyl)ethynyl]-5-iodobenzene

Downstream raw materials:

2,5-bis(dodecyloxy)-4-(2'-ethynyl)triisopropylsilylacetylenylbenzene

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