2,4,6-Tris(4-ethynylphenyl)-1,3,5-triazine

Base Information

Chemical Name:2,4,6-Tris(4-ethynylphenyl)-1,3,5-triazine
CAS No.:425629-22-7
Molecular Formula:C₂₇H₁₅N₃
Molecular Weight:381.436
Hs Code.:

Synonyms:2,4,6-tris[(4-ethynyl)phenyl]-1,3,5-triazine

Suppliers and Price of 2,4,6-Tris(4-ethynylphenyl)-1,3,5-triazine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Arctom
2,4,6-Tris(4-ethynylphenyl)-1,3,5-triazine 98%
1g
$ 295.00

Arctom
2,4,6-Tris(4-ethynylphenyl)-1,3,5-triazine 98%
250mg
$ 112.00

Arctom
2,4,6-Tris(4-ethynylphenyl)-1,3,5-triazine 98%
100mg
$ 75.00

Total 22 raw suppliers

Chemical Property of 2,4,6-Tris(4-ethynylphenyl)-1,3,5-triazine

Chemical Property:

Boiling Point:593.6±60.0 °C(Predicted)
PKA:0.02±0.10(Predicted)
Density:1.28±0.1 g/cm3(Predicted)

Purity/Quality:

99% ^*data from raw suppliers

2,4,6-Tris(4-ethynylphenyl)-1,3,5-triazine 98% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2,4,6-Tris(4-ethynylphenyl)-1,3,5-triazine

There total 2 articles about 2,4,6-Tris(4-ethynylphenyl)-1,3,5-triazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 2,4,6-tris{4-[(trimethylsilyl)ethynyl]-phenyl}-1,3,5-triazine

: 425629-22-7
2,4,6-tris[(4-ethynyl)phenyl]-1,3,5-triazine

Guidance literature:: With potassium carbonate; In methanol; at 20 ℃; for 24h;
DOI:10.3390/molecules24193480

Reference yield:

: 30363-03-2
2,4,6-tris(4-bromophenyl)-1,3,5-triazine

: 425629-22-7
2,4,6-tris[(4-ethynyl)phenyl]-1,3,5-triazine

Guidance literature:: Multi-step reaction with 2 steps

1: Pd(PPh₃)4; CuI; triethylamine / tetrahydrofuran / 55 °C

2: tetrabutylammonium fluoride / tetrahydrofuran / 20 °C

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetrabutyl ammonium fluoride; triethylamine; In tetrahydrofuran;
DOI:10.1246/bcsj.75.615

Reference yield: 98.0%

: cis-[RuCl2(dppe)2]

: 425629-22-7
2,4,6-tris[(4-ethynyl)phenyl]-1,3,5-triazine

: 2,4,6-[4-(Cl(dppe)2RuCC)C₆H₄]3-1,3,5-C₃N₃

Guidance literature:: With NEt₃; NaPF₆; In dichloromethane; under N2; equimolar mixt. of Ru complex and NaPF6 in CH2Cl2 stirred at room temp. for 2 h; ligand (0.27 equiv.) in CH2Cl2 slowly added over 2 h;stirred overnight; NEt3 added; stirred for 30 min; solvent removed under vac.; extd. with benzene; filtered through Celite;solvent removed; washed with MeOH; recrystd. from CH2Cl2-hexane; dried under vac. overnight; elem. anal.;
DOI:10.1021/om0502133