Technology Process of 3-(dibenzothiophen-4-yl)-9-(9,10-diphenyl-2-anthryl)-9H-carbazole
There total 3 articles about 3-(dibenzothiophen-4-yl)-9-(9,10-diphenyl-2-anthryl)-9H-carbazole which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium t-butanolate;
tri-tert-butyl phosphine; bis(dibenzylideneacetone)-palladium(0);
In
hexane; toluene;
at 110 ℃;
for 4h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium carbonate / palladium diacetate; tris-(o-tolyl)phosphine / toluene; ethanol; water / 3 h / 110 °C / Inert atmosphere
2: sodium t-butanolate / bis(dibenzylideneacetone)-palladium(0); tri-tert-butyl phosphine / toluene; hexane / 4 h / 110 °C / Inert atmosphere
With
potassium carbonate; sodium t-butanolate;
tri-tert-butyl phosphine; palladium diacetate; tris-(o-tolyl)phosphine; bis(dibenzylideneacetone)-palladium(0);
In
ethanol; hexane; water; toluene;
1: Suzuki-Miyaura Coupling / 2: Buchwald-Hartwig Reaction;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium carbonate / palladium diacetate; tris-(o-tolyl)phosphine / toluene; ethanol; water / 3 h / 110 °C / Inert atmosphere
2: sodium t-butanolate / bis(dibenzylideneacetone)-palladium(0); tri-tert-butyl phosphine / toluene; hexane / 4 h / 110 °C / Inert atmosphere
With
potassium carbonate; sodium t-butanolate;
tri-tert-butyl phosphine; palladium diacetate; tris-(o-tolyl)phosphine; bis(dibenzylideneacetone)-palladium(0);
In
ethanol; hexane; water; toluene;
1: Suzuki-Miyaura Coupling / 2: Buchwald-Hartwig Reaction;