E-1-(4-((5'-(6-oxo-5-thiaheptylsulfanyl)-2,2'-bithiophene-5-sulfanyl)methyl)phenyl)-2-p-tolyldiazene

Base Information

• Chemical Name: E-1-(4-((5'-(6-oxo-5-thiaheptylsulfanyl)-2,2'-bithiophene-5-sulfanyl)methyl)phenyl)-2-p-tolyldiazene
• CAS No.: 1234871-32-9
• Molecular Formula: C₂₈H₂₈N₂OS₅
• Molecular Weight: 568.873

Synonyms:E-1-(4-((5'-(6-oxo-5-thiaheptylsulfanyl)-2,2'-bithiophene-5-sulfanyl)methyl)phenyl)-2-p-tolyldiazene

Chemical Property of E-1-(4-((5'-(6-oxo-5-thiaheptylsulfanyl)-2,2'-bithiophene-5-sulfanyl)methyl)phenyl)-2-p-tolyldiazene

Chemical Property:

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Technology Process of E-1-(4-((5'-(6-oxo-5-thiaheptylsulfanyl)-2,2'-bithiophene-5-sulfanyl)methyl)phenyl)-2-p-tolyldiazene

There total 1 articles about E-1-(4-((5'-(6-oxo-5-thiaheptylsulfanyl)-2,2'-bithiophene-5-sulfanyl)methyl)phenyl)-2-p-tolyldiazene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

thioacetic acid S-(4-bromo-butyl)ester (14475-59-3) + C22H18N2S4 → E-1-(4-((5'-(6-oxo-5-thiaheptylsulfanyl)-2,2'-bithiophene-5-sulfanyl)methyl)phenyl)-2-p-tolyldiazene (1234871-32-9)

Guidance literature:

In methanol; N,N-dimethyl-formamide; Inert atmosphere;

DOI:10.1039/c002072a

Reference yield: 80.0%

E-1-(4-((5'-(6-oxo-5-thiaheptylsulfanyl)-2,2'-bithiophene-5-sulfanyl)methyl)phenyl)-2-p-tolyldiazene (1234871-32-9) → E-1-(4-((5'-(4-mercaptobutylsulfanyl)-2,2'-bithiophene-5-sulfanyl)methyl)phenyl)-2-p-tolyldiazene (1234871-19-2)

Guidance literature:

E-1-(4-((5'-(6-oxo-5-thiaheptylsulfanyl)-2,2'-bithiophene-5-sulfanyl)methyl)phenyl)-2-p-tolyldiazene; With cesiumhydroxide monohydrate; In tetrahydrofuran; methanol; at 20 ℃; Inert atmosphere;

With hydrogenchloride; In tetrahydrofuran; methanol; water; for 2h; Inert atmosphere;

DOI:10.1039/c002072a

Reference yield:

E-1-(4-((5'-(6-oxo-5-thiaheptylsulfanyl)-2,2'-bithiophene-5-sulfanyl)methyl)phenyl)-2-p-tolyldiazene (1234871-32-9) → 1-(4-((5'-(6-oxo-5-thiaheptylsulfanyl)-2,2'-bithiophene-5-sulfanyl)methyl)phenyl)-2-p-tolyldiazene

Guidance literature:

In dichloromethane; at 20 ℃; for 1h; UV-irradiation;

DOI:10.1039/c002072a

upstream raw materials:

thioacetic acid S-(4-bromo-butyl)ester

Downstream raw materials:

E-1-(4-((5'-(4-mercaptobutylsulfanyl)-2,2'-bithiophene-5-sulfanyl)methyl)phenyl)-2-p-tolyldiazene

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