<3--1,3,5-triazin-2-yl>amino>-5-bromobenzoyl>-N-<<4-(1,1-dimethylethyl)phenyl>methyl>amino>phenyl>carbamic acid 1,1-dimethylethyl ester

Base Information

Chemical Name:<3--1,3,5-triazin-2-yl>amino>-5-bromobenzoyl>-N-<<4-(1,1-dimethylethyl)phenyl>methyl>amino>phenyl>carbamic acid 1,1-dimethylethyl ester
CAS No.:147355-08-6
Molecular Formula:C₃₈H₄₉BrN₈O₃
Molecular Weight:745.763
Hs Code.:

<3-<N-<2-<<4-amino-6-<(3,3-dimethylbutyl)amino>-1,3,5-triazin-2-yl>amino>-5-bromobenzoyl>-N-<<4-(1,1-dimethylethyl)phenyl>methyl>amino>phenyl>carbamic acid 1,1-dimethylethyl ester

Synonyms:<3--1,3,5-triazin-2-yl>amino>-5-bromobenzoyl>-N-<<4-(1,1-dimethylethyl)phenyl>methyl>amino>phenyl>carbamic acid 1,1-dimethylethyl ester

Suppliers and Price of <3--1,3,5-triazin-2-yl>amino>-5-bromobenzoyl>-N-<<4-(1,1-dimethylethyl)phenyl>methyl>amino>phenyl>carbamic acid 1,1-dimethylethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of <3--1,3,5-triazin-2-yl>amino>-5-bromobenzoyl>-N-<<4-(1,1-dimethylethyl)phenyl>methyl>amino>phenyl>carbamic acid 1,1-dimethylethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of <3--1,3,5-triazin-2-yl>amino>-5-bromobenzoyl>-N-<<4-(1,1-dimethylethyl)phenyl>methyl>amino>phenyl>carbamic acid 1,1-dimethylethyl ester

There total 11 articles about <3--1,3,5-triazin-2-yl>amino>-5-bromobenzoyl>-N-<<4-(1,1-dimethylethyl)phenyl>methyl>amino>phenyl>carbamic acid 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 15673-00-4
3,3-dimethylbutylamine

: 147355-07-5
<3--5-bromobenzoyl>-N-<<4-(1,1-dimethylethyl)phenyl>methyl>amino>phenyl>carbamic acid 1,1-dimethylethyl ester

: 147355-08-6
<3--1,3,5-triazin-2-yl>amino>-5-bromobenzoyl>-N-<<4-(1,1-dimethylethyl)phenyl>methyl>amino>phenyl>carbamic acid 1,1-dimethylethyl ester

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; for 4h; Heating;
DOI:10.1021/ja00056a014

Reference yield:

: 68621-88-5
(3-aminophenyl)carbamic acid tert-butyl ester

: 147355-08-6
<3--1,3,5-triazin-2-yl>amino>-5-bromobenzoyl>-N-<<4-(1,1-dimethylethyl)phenyl>methyl>amino>phenyl>carbamic acid 1,1-dimethylethyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: 68 percent / triethylamine / tetrahydrofuran / 12 h / Heating

2: 90 percent / triethylamine / CH₂Cl₂; toluene / 1 h / Ambient temperature

3: 95 percent / hydrazine / methanol / 4 h / Heating

4: diisopropylethylamine / tetrahydrofuran / 1 h / 0 °C

5: NH₃ gas / tetrahydrofuran / 1 h / 0 °C

6: 86 percent / diisopropylethylamine / tetrahydrofuran / 4 h / Heating

With ammonia; triethylamine; N-ethyl-N,N-diisopropylamine; hydrazine; In tetrahydrofuran; methanol; dichloromethane; toluene;
DOI:10.1021/ja00056a014

Reference yield:

: 147355-04-2
5-bromo-2-(1,3-dihydro-1,3-dioxo-2H-isoindol-2-yl)benzoic acid

: 147355-08-6
<3--1,3,5-triazin-2-yl>amino>-5-bromobenzoyl>-N-<<4-(1,1-dimethylethyl)phenyl>methyl>amino>phenyl>carbamic acid 1,1-dimethylethyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: thionyl chloride / 2 h / Heating

2: 90 percent / triethylamine / CH₂Cl₂; toluene / 1 h / Ambient temperature

3: 95 percent / hydrazine / methanol / 4 h / Heating

4: diisopropylethylamine / tetrahydrofuran / 1 h / 0 °C

5: NH₃ gas / tetrahydrofuran / 1 h / 0 °C

6: 86 percent / diisopropylethylamine / tetrahydrofuran / 4 h / Heating

With thionyl chloride; ammonia; triethylamine; N-ethyl-N,N-diisopropylamine; hydrazine; In tetrahydrofuran; methanol; dichloromethane; toluene;
DOI:10.1021/ja00056a014