C₁₇H₁₄BrNO₂

Base Information

Chemical Name:C₁₇H₁₄BrNO₂
CAS No.:1310372-99-6
Molecular Formula:C₁₇H₁₄BrNO₂
Molecular Weight:344.208
Hs Code.:

C<sub>17</sub>H<sub>14</sub>BrNO<sub>2</sub>

Synonyms:C₁₇H₁₄BrNO₂

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Chemical Property of C₁₇H₁₄BrNO₂

Chemical Property:

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Technology Process of C₁₇H₁₄BrNO₂

There total 3 articles about C₁₇H₁₄BrNO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 696-62-8
para-iodoanisole

: 267408-61-7
N-(2'-Bromophenyl)-N-methylpropynamide

: 1310372-99-6
C₁₇H₁₄BrNO₂

Guidance literature:: With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium acetate; In N,N-dimethyl-formamide; at 25 - 60 ℃; for 1h; Inert atmosphere;
DOI:10.1055/s-0033-1339690

Reference yield:

: 615-36-1
2-bromoaniline

: 1310372-99-6
C₁₇H₁₄BrNO₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: dicyclohexyl-carbodiimide / dichloromethane / 12 h / 0 - 20 °C / Inert atmosphere

2.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 °C / Inert atmosphere

2.2: 6 h / 0 - 25 °C / Inert atmosphere

3.1: copper(l) iodide; sodium acetate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide / 1 h / 25 - 60 °C / Inert atmosphere

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium acetate; sodium hydride; dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; mineral oil; 3.1: |Sonogashira Cross-Coupling;
DOI:10.1055/s-0033-1339690

Reference yield:

: 267408-59-3
N-(2'-Bromophenyl)propynamide

: 1310372-99-6
C₁₇H₁₄BrNO₂

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 °C / Inert atmosphere

1.2: 6 h / 0 - 25 °C / Inert atmosphere

2.1: copper(l) iodide; sodium acetate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide / 1 h / 25 - 60 °C / Inert atmosphere

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium acetate; sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide; mineral oil; 2.1: |Sonogashira Cross-Coupling;
DOI:10.1055/s-0033-1339690