2-Methoxy-5-(5,6,8,9-tetrahydro-dibenzo[c,h]acridin-7-yl)-benzenesulfonic acid; compound with perchloric acid

Base Information

Chemical Name:2-Methoxy-5-(5,6,8,9-tetrahydro-dibenzo[c,h]acridin-7-yl)-benzenesulfonic acid; compound with perchloric acid
CAS No.:92445-40-4
Molecular Formula:C₂₈H₂₃NO₄S*ClHO₄
Molecular Weight:570.019
Hs Code.:

Synonyms:2-Methoxy-5-(5,6,8,9-tetrahydro-dibenzo[c,h]acridin-7-yl)-benzenesulfonic acid; compound with perchloric acid

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Chemical Property of 2-Methoxy-5-(5,6,8,9-tetrahydro-dibenzo[c,h]acridin-7-yl)-benzenesulfonic acid; compound with perchloric acid

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Technology Process of 2-Methoxy-5-(5,6,8,9-tetrahydro-dibenzo[c,h]acridin-7-yl)-benzenesulfonic acid; compound with perchloric acid

There total 10 articles about 2-Methoxy-5-(5,6,8,9-tetrahydro-dibenzo[c,h]acridin-7-yl)-benzenesulfonic acid; compound with perchloric acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 5,6,8,9-tetrahydro-7-(4-methoxy-3-sulphophenyl)dibenzo-xanthylium perchlorate

: 92445-40-4
2-Methoxy-5-(5,6,8,9-tetrahydro-dibenzo[c,h]acridin-7-yl)-benzenesulfonic acid; compound with perchloric acid

Guidance literature:: With ammonia; In water;

Reference yield:

: 79-46-9
2-nitropropane

: 14-(1-ammonio-1-carboxypentyl)-5,6,8,9-tetrahydro-7-(4-methoxy-3-sulphonatophenyl)dibenzoacridinium perchlorate

: 92445-40-4
2-Methoxy-5-(5,6,8,9-tetrahydro-dibenzo[c,h]acridin-7-yl)-benzenesulfonic acid; compound with perchloric acid

: 4043-87-2,83680-83-5
pipecolic Acid

Guidance literature:: With sodium hydride; Yield given. Multistep reaction; 1.) water, 25 deg C, 10 min; 2.) water, 80 deg C, 3 h; further solv., var. temp. and time;

Reference yield:

: 529-34-0
3,4-dihydronaphthalene-1(2H)-one

: 92445-40-4
2-Methoxy-5-(5,6,8,9-tetrahydro-dibenzo[c,h]acridin-7-yl)-benzenesulfonic acid; compound with perchloric acid

Guidance literature:: Multi-step reaction with 3 steps

1: 39 percent / 70 percent perchloric acid, acetic anhydrid / 100 °C

2: 39 percent / sodium hydroxide / H₂O; ethanol / 48 h / 25 °C / pH 10-10.2 (10 M NaOH)

3: 1.) sodium hydride / 1.) water, 25 deg C, 10 min; 2.) water, 80 deg C, 1 h

With sodium hydroxide; perchloric acid; acetic anhydride; sodium hydride; In ethanol; water;