[2-(4-isocyanatophenoxycarbonylmethoxy)ethoxy]acetic acid 4-isocyanatophenyl ester

Base Information

Chemical Name:[2-(4-isocyanatophenoxycarbonylmethoxy)ethoxy]acetic acid 4-isocyanatophenyl ester
CAS No.:1609647-63-3
Molecular Formula:C₂₀H₁₆N₂O₈
Molecular Weight:412.356
Hs Code.:

Synonyms:[2-(4-isocyanatophenoxycarbonylmethoxy)ethoxy]acetic acid 4-isocyanatophenyl ester

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Chemical Property of [2-(4-isocyanatophenoxycarbonylmethoxy)ethoxy]acetic acid 4-isocyanatophenyl ester

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Technology Process of [2-(4-isocyanatophenoxycarbonylmethoxy)ethoxy]acetic acid 4-isocyanatophenyl ester

There total 4 articles about [2-(4-isocyanatophenoxycarbonylmethoxy)ethoxy]acetic acid 4-isocyanatophenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 32315-10-9
bis(trichloromethyl) carbonate

: 1609647-62-2
[2-(4-aminophenoxycarbonylmethoxy)ethoxy]acetic acid 4-aminophenyl ester

: 1609647-63-3
[2-(4-isocyanatophenoxycarbonylmethoxy)ethoxy]acetic acid 4-isocyanatophenyl ester

Guidance literature:: In 1,4-dioxane; at 10 - 85 ℃; for 2h; Inert atmosphere;

Reference yield:

: 100-02-7,78813-13-5,89830-32-0
4-nitro-phenol

: 1609647-63-3
[2-(4-isocyanatophenoxycarbonylmethoxy)ethoxy]acetic acid 4-isocyanatophenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: benzotriazol-1-ol; dicyclohexyl-carbodiimide / tetrahydrofuran / 36 h / 0 - 20 °C / Inert atmosphere

2: hydrogen; 5%-palladium/activated carbon / N,N-dimethyl-formamide / 1 h / Autoclave

3: 1,4-dioxane / 2 h / 10 - 85 °C / Inert atmosphere

With 5%-palladium/activated carbon; hydrogen; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In tetrahydrofuran; 1,4-dioxane; N,N-dimethyl-formamide;

Reference yield:

: [2-(4-nitrophenoxycarbonylmethoxy)ethoxy]acetic acid 4-nitrophenyl ester

: 1609647-63-3
[2-(4-isocyanatophenoxycarbonylmethoxy)ethoxy]acetic acid 4-isocyanatophenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen; 5%-palladium/activated carbon / N,N-dimethyl-formamide / 1 h / Autoclave

2: 1,4-dioxane / 2 h / 10 - 85 °C / Inert atmosphere

With 5%-palladium/activated carbon; hydrogen; In 1,4-dioxane; N,N-dimethyl-formamide;