methyl-2 (methyl-2' dithianyl)-4 cyclohexene-1 carboxylate de methyle

Base Information

Chemical Name:methyl-2 (methyl-2' dithianyl)-4 cyclohexene-1 carboxylate de methyle
CAS No.:82792-73-2
Molecular Formula:C₁₄H₂₂O₂S₂
Molecular Weight:286.459
Hs Code.:

Synonyms:methyl-2 (methyl-2' dithianyl)-4 cyclohexene-1 carboxylate de methyle

Suppliers and Price of methyl-2 (methyl-2' dithianyl)-4 cyclohexene-1 carboxylate de methyle

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of methyl-2 (methyl-2' dithianyl)-4 cyclohexene-1 carboxylate de methyle

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of methyl-2 (methyl-2' dithianyl)-4 cyclohexene-1 carboxylate de methyle

There total 6 articles about methyl-2 (methyl-2' dithianyl)-4 cyclohexene-1 carboxylate de methyle which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 930-68-7
cyclohexenone

: 82792-73-2
methyl-2 (methyl-2' dithianyl)-4 cyclohexene-1 carboxylate de methyle

Guidance literature:: Multi-step reaction with 3 steps

1: tetrahydrofuran; hexamethylphosphoric acid triamide / -78 °C

2: NaH, cat. MeOH / benzene / Heating

3: 1.) NaH, (EtO)2POCl / 1.) THF, 20 deg C, 1 h, 2.) ether, -78 to 20 deg C

With methanol; sodium hydride; diethyl chlorophosphate; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; benzene;
DOI:10.1039/c39820000421

Reference yield:

: 68984-52-1
3-[2-(2-methyl-1,3-dithianyl)]-cyclohexanone

: 82792-73-2
methyl-2 (methyl-2' dithianyl)-4 cyclohexene-1 carboxylate de methyle

Guidance literature:: Multi-step reaction with 2 steps

1: NaH, cat. MeOH / benzene / Heating

2: 1.) NaH, (EtO)2POCl / 1.) THF, 20 deg C, 1 h, 2.) ether, -78 to 20 deg C

With methanol; sodium hydride; diethyl chlorophosphate; In benzene;
DOI:10.1039/c39820000421

Reference yield:

: 27969-97-7
2-lithio-2-methyl-1,3-dithiane

: 82792-73-2
methyl-2 (methyl-2' dithianyl)-4 cyclohexene-1 carboxylate de methyle

Guidance literature:: Multi-step reaction with 3 steps

1: tetrahydrofuran; hexamethylphosphoric acid triamide / -78 °C

2: NaH, cat. MeOH / benzene / Heating

3: 1.) NaH, (EtO)2POCl / 1.) THF, 20 deg C, 1 h, 2.) ether, -78 to 20 deg C

With methanol; sodium hydride; diethyl chlorophosphate; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; benzene;
DOI:10.1039/c39820000421