C₁₁H₁₅BrO

Base Information

• Chemical Name: C₁₁H₁₅BrO
• CAS No.: 1342886-82-1
• Molecular Formula: C₁₁H₁₅BrO
• Molecular Weight: 243.143
• Mol file: 1342886-82-1.mol

Synonyms:C₁₁H₁₅BrO

Chemical Property of C₁₁H₁₅BrO

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₁H₁₅BrO

There total 2 articles about C₁₁H₁₅BrO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-bromo-2-methyl-1-phenylbutan-1-one (873998-30-2) → C11H15BrO (1342886-82-1)

Guidance literature:

With methanol; sodium tetrahydroborate; at 0 ℃; Inert atmosphere;

DOI:10.1016/j.tetlet.2011.08.134

Reference yield:

2-methyl-1-phenyl-butan-1-one (938-87-4) → C11H15BrO (1342886-82-1)

Guidance literature:

Multi-step reaction with 2 steps

1: bromine; acetic acid / Inert atmosphere; Reflux

2: methanol; sodium tetrahydroborate / 0 °C / Inert atmosphere

With methanol; sodium tetrahydroborate; bromine; acetic acid;

DOI:10.1016/j.tetlet.2011.08.134

Reference yield:

C11H15BrO (1342886-82-1) → 2-methyl-2-phenylbutyraldehyde (4370-86-9) + 2-methyl-1-phenyl-butan-1-one (938-87-4)

Guidance literature:

With diethylzinc; trifluoroacetic acid; In dichloromethane; at 20 ℃; for 1h; Inert atmosphere;

DOI:10.1016/j.tetlet.2011.08.134

upstream raw materials:

2-bromo-2-methyl-1-phenylbutan-1-one

2-methyl-1-phenyl-butan-1-one

Downstream raw materials:

2-methyl-2-phenylbutyraldehyde

2-methyl-1-phenyl-butan-1-one