(C₄H₉)4N⁽¹⁺⁾*[((CO)5Cr)2Sn(C₅H₇O₂)]^(1-)=[(C₄H₉)4N][((CO)5Cr)2Sn(C₅H₇O₂)]

Base Information

• Chemical Name: (C₄H₉)4N⁽¹⁺⁾*[((CO)5Cr)2Sn(C₅H₇O₂)]^(1-)=[(C₄H₉)4N][((CO)5Cr)2Sn(C₅H₇O₂)]
• CAS No.: 212562-32-8
• Molecular Formula: C₁₅H₇Cr₂O₁₂Sn*C₁₆H₃₆N
• Molecular Weight: 844.384
• Mol file: 212562-32-8.mol

Synonyms:(C₄H₉)4N⁽¹⁺⁾*[((CO)5Cr)2Sn(C₅H₇O₂)]^(1-)=[(C₄H₉)4N][((CO)5Cr)2Sn(C₅H₇O₂)]

Chemical Property of (C₄H₉)4N⁽¹⁺⁾*[((CO)5Cr)2Sn(C₅H₇O₂)]^(1-)=[(C₄H₉)4N][((CO)5Cr)2Sn(C₅H₇O₂)]

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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Useful:

Technology Process of (C₄H₉)4N⁽¹⁺⁾*[((CO)5Cr)2Sn(C₅H₇O₂)]^(1-)=[(C₄H₉)4N][((CO)5Cr)2Sn(C₅H₇O₂)]

There total 1 articles about (C₄H₉)4N⁽¹⁺⁾*[((CO)5Cr)2Sn(C₅H₇O₂)]^(1-)=[(C₄H₉)4N][((CO)5Cr)2Sn(C₅H₇O₂)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

2(C4H9)4N(1+)*[((CO)5Cr)2Sn(OC2H5)]2(2-)=[(C4H9)4N]2[[((CO)5Cr)2Sn(OC2H5)]2] + acetylacetone (123-54-6,81235-32-7) → (C4H9)4N(1+)*[((CO)5Cr)2Sn(C5H7O2)](1-)=[(C4H9)4N][((CO)5Cr)2Sn(C5H7O2)] (212562-32-8) + chromium(0) hexacarbonyl (199620-14-9,13007-92-6)

Guidance literature:

In tetrahydrofuran; byproducts: CH3CH2OH; Ar atmosphere, addn. of pentanedione to soln. of tin compound at 25°C, stirring (2 h); filtration (Kieselgur), drying, dissolution (THF), chromy. (silica gel, elution of Cr(CO)6 with Et2O, elution of tin complex with THF), evapn. of solvent (vacuum);

DOI:10.1002/(sici)1099-0682(199808)1998:8<1057::aid-ejic1057>3.0.co;2-9

upstream raw materials:

acetylacetone