4-Chloro-3-methoxy-2-methylpyridine N-oxide

Base Information

Chemical Name:4-Chloro-3-methoxy-2-methylpyridine N-oxide
CAS No.:122307-41-9
Molecular Formula:C7H8ClNO2
Molecular Weight:173.599
Hs Code.:2933399990
European Community (EC) Number:602-491-2
DSSTox Substance ID:DTXSID10408154
Nikkaji Number:J2.485.368C
Wikidata:Q72453194
Mol file:122307-41-9.mol

Synonyms:4-Chloro-3-methoxy-2-methylpyridine N-oxide;122307-41-9;4-Chloro-3-methoxy-2-methylpyridine 1-oxide;Pyridine, 4-chloro-3-methoxy-2-methyl-, 1-oxide;4-chloro-3-methoxy-2-methyl-1-oxidopyridin-1-ium;2-methyl-3-methoxy-4-chloropyridine N-oxide;MFCD03093995;4-Chloro-2-methyl-3-methoxypyridine N-oxide;EC 602-491-2;SCHEMBL317432;DTXSID10408154;TWXMQDRFBLSXFN-UHFFFAOYSA-N;AMY37202;ZB1366;AKOS015891516;AC-8440;AS-10872;SY018469;4-Chloro-3-methoxy-2-methylpyridine1-oxide;C2402;FT-0642982;NS00004558;4-Chloro-2-methyl-3-methoxypyridine N-Oxide;F12227;A804870;4-Chloro-3-methoxy-2-methylpyridine N-oxide, 97%;Q-200452

Suppliers and Price of 4-Chloro-3-methoxy-2-methylpyridine N-oxide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Usbiological
4-Chloro-3-methoxy-2-methylpyridine N-Oxide
1g
$ 312.00

Usbiological
4-Chloro-3-methoxy-2-methylpyridine N-oxide
10g
$ 305.00

TRC
4-Chloro-3-methoxy-2-methylpyridine N-Oxide
1g
$ 65.00

TCI Chemical
4-Chloro-3-methoxy-2-methylpyridine N-Oxide >98.0%(GC)
25g
$ 321.00

TCI Chemical
4-Chloro-3-methoxy-2-methylpyridine N-Oxide >98.0%(GC)
5g
$ 106.00

SynQuest Laboratories
4-Chloro-3-methoxy-2-methylpyridine N-oxide
5 g
$ 32.00

SynQuest Laboratories
4-Chloro-3-methoxy-2-methylpyridine N-oxide
25 g
$ 144.00

Sigma-Aldrich
4-Chloro-3-methoxy-2-methylpyridine N-oxide 97%
25g
$ 292.00

Matrix Scientific
4-Chloro-3-methoxy-2-methylpyridine 1-oxide 97%
1g
$ 47.00

Matrix Scientific
4-Chloro-3-methoxy-2-methylpyridine 1-oxide 97%
10g
$ 110.00

Total 66 raw suppliers

Chemical Property of 4-Chloro-3-methoxy-2-methylpyridine N-oxide

Chemical Property:

Appearance/Colour:off-white solid
Vapor Pressure:0.000117mmHg at 25°C
Melting Point:96-100 °C(lit.)
Refractive Index:1.527
Boiling Point:346.2 °C at 760 mmHg
PKA:1.14±0.10(Predicted)
Flash Point:163.2 °C
PSA：34.69000
Density:1.25 g/cm³
LogP:2.08550
Storage Temp.:Inert atmosphere,Room Temperature
Solubility.:Ethyl Acetate (Slightly), Methanol (Slightly), Water (Slightly)
XLogP3:0.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:173.0243562
Heavy Atom Count:11
Complexity:134

Purity/Quality:

99% ^*data from raw suppliers

4-Chloro-3-methoxy-2-methylpyridine N-Oxide ^*data from reagent suppliers

Safty Information:

Pictogram(s): Xi
Hazard Codes:Xi
Statements: 36/37/38
Safety Statements: 26-36

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=[N+](C=CC(=C1OC)Cl)[O-]
Uses 4-Chloro-3-methoxy-2-methylpyridine N-oxide (cas# 122307-41-9) is a compound useful in organic synthesis.

Technology Process of 4-Chloro-3-methoxy-2-methylpyridine N-oxide

There total 3 articles about 4-Chloro-3-methoxy-2-methylpyridine N-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 107512-34-5
4-Chloro-3-methoxy-2-methyl-pyridine

: 122307-41-9
4-chloro-3-methoxy-2-methylpyridine N-oxide

Guidance literature:: With phosphotungstic acid; dihydrogen peroxide; In water; at 85 - 87 ℃; for 5h; Temperature;

Reference yield:

: 76015-11-7
3-methoxy-2-methylpyridin-4(1H)-one

: 122307-41-9
4-chloro-3-methoxy-2-methylpyridine N-oxide

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / POCl₃ / 18 h / 90 °C

2: 90 percent / 30percent aq. H₂O₂, AcOH / 24 h / 90 °C

With dihydrogen peroxide; acetic acid; trichlorophosphate;
DOI:10.1021/jm00084a010