4-(3-bromo-5-nitrobenzyl)-2,6-dimethylmorpholine

Base Information

Chemical Name:4-(3-bromo-5-nitrobenzyl)-2,6-dimethylmorpholine
CAS No.:1202036-22-3
Molecular Formula:C₁₃H₁₇BrN₂O₃
Molecular Weight:329.194
Hs Code.:

Synonyms:4-(3-bromo-5-nitrobenzyl)-2,6-dimethylmorpholine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-(3-bromo-5-nitrobenzyl)-2,6-dimethylmorpholine

Chemical Property:

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Technology Process of 4-(3-bromo-5-nitrobenzyl)-2,6-dimethylmorpholine

There total 2 articles about 4-(3-bromo-5-nitrobenzyl)-2,6-dimethylmorpholine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6307-83-1
3-bromo-5-nitro-benzoic acid

: 1202036-22-3
4-(3-bromo-5-nitrobenzyl)-2,6-dimethylmorpholine

Guidance literature:: Multi-step reaction with 2 steps

1.1: borane-THF / tetrahydrofuran / 0 - 20 °C

1.2: 0 °C

2.1: methanesulfonyl chloride; triethylamine / dichloromethane / 0 - 20 °C

2.2: 16 h / 20 °C

With borane-THF; methanesulfonyl chloride; triethylamine; In tetrahydrofuran; dichloromethane;

Reference yield:

: 141-91-3
2,6-dimethyl morpholine

: 139194-79-9
(3-bromo-5-nitrophenyl)methanol

: 1202036-22-3
4-(3-bromo-5-nitrobenzyl)-2,6-dimethylmorpholine

Guidance literature:: (3-bromo-5-nitrophenyl)methanol; With methanesulfonyl chloride; triethylamine; In dichloromethane; at 0 - 20 ℃;

2,6-dimethyl morpholine; In dichloromethane; at 20 ℃; for 16h;

Reference yield:

: 1202036-22-3
4-(3-bromo-5-nitrobenzyl)-2,6-dimethylmorpholine

: 761446-44-0
1-methyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-pyrazole

: 1202036-23-4
2,6-dimethyl-4-(3-(1-methyl-1H-pyrazol-4-yl)-5-nitrobenzyl)morpholine

Guidance literature:: With sodium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In 1,2-dimethoxyethane; water; at 120 ℃; for 0.166667h;