3,5-dimethoxy-1-(1-heptylcyclopropyl)benzene

Base Information

Chemical Name:3,5-dimethoxy-1-(1-heptylcyclopropyl)benzene
CAS No.:951039-72-8
Molecular Formula:C₁₈H₂₈O₂
Molecular Weight:276.419
Hs Code.:

Synonyms:3,5-dimethoxy-1-(1-heptylcyclopropyl)benzene

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Chemical Property of 3,5-dimethoxy-1-(1-heptylcyclopropyl)benzene

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Technology Process of 3,5-dimethoxy-1-(1-heptylcyclopropyl)benzene

There total 4 articles about 3,5-dimethoxy-1-(1-heptylcyclopropyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 951039-66-0
3,5-dimethoxy-1-[1-[(1Z)-1-heptenyl]cyclopropyl]benzene

: 951039-72-8
3,5-dimethoxy-1-(1-heptylcyclopropyl)benzene

Guidance literature:: With toluene-4-sulfonic acid hydrazide; In acetate buffer; N,N-dimethyl-formamide; for 12h; Heating;
DOI:10.1021/jm070121a

Reference yield:

: 13388-75-5
3,5-dimethoxyphenylacetonitrile

: 951039-72-8
3,5-dimethoxy-1-(1-heptylcyclopropyl)benzene

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium bis(trimethylsilyl)amide / tetrahydrofuran / -16 °C

1.2: 62 percent / tetrahydrofuran / 3 h / 0 °C

2.1: 98 percent / diisobutylaluminum hydride / CH₂Cl₂ / 0.75 h / -78 °C

3.1: bis(trimethylsilyl)amide / tetrahydrofuran / 0 - 10 °C

3.2: 80 percent / tetrahydrofuran / 0.75 h / 10 °C

4.1: 76 percent / p-toluenesulfonhydrazide / dimethylformamide; acetate buffer / 12 h / Heating

With hexamethyldisilazide; potassium hexamethylsilazane; diisobutylaluminium hydride; toluene-4-sulfonic acid hydrazide; In tetrahydrofuran; dichloromethane; acetate buffer; N,N-dimethyl-formamide;
DOI:10.1021/jm070121a

Reference yield:

: 124276-97-7
1-(3,5-dimethoxyphenyl)cyclopropanecarbonitrile

: 951039-72-8
3,5-dimethoxy-1-(1-heptylcyclopropyl)benzene

Guidance literature:: Multi-step reaction with 3 steps

1.1: 98 percent / diisobutylaluminum hydride / CH₂Cl₂ / 0.75 h / -78 °C

2.1: bis(trimethylsilyl)amide / tetrahydrofuran / 0 - 10 °C

2.2: 80 percent / tetrahydrofuran / 0.75 h / 10 °C

3.1: 76 percent / p-toluenesulfonhydrazide / dimethylformamide; acetate buffer / 12 h / Heating

With hexamethyldisilazide; diisobutylaluminium hydride; toluene-4-sulfonic acid hydrazide; In tetrahydrofuran; dichloromethane; acetate buffer; N,N-dimethyl-formamide;
DOI:10.1021/jm070121a