α-hydroxy-2,5-dihydrocumene

Base Information

Chemical Name:α-hydroxy-2,5-dihydrocumene
CAS No.:77023-04-2
Molecular Formula:C₉H₁₄O
Molecular Weight:138.21
Hs Code.:

Synonyms:α-hydroxy-2,5-dihydrocumene

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Chemical Property of α-hydroxy-2,5-dihydrocumene

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Technology Process of α-hydroxy-2,5-dihydrocumene

There total 2 articles about α-hydroxy-2,5-dihydrocumene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 50983-21-6
1,4-Cyclohexadien-1-carbonsaeure-methylester

: 917-54-4
methyllithium

: 77023-04-2
α-hydroxy-2,5-dihydrocumene

Guidance literature:: In diethyl ether; for 1h; Ambient temperature;
DOI:10.1021/ja00394a029

Reference yield:

: 917-64-6
methyl magnesium iodide

: 102872-23-1
1-acetyl-1,4-cyclohexadiene

: 77023-04-2
α-hydroxy-2,5-dihydrocumene

Guidance literature:: With diethyl ether;

Reference yield:

: 77023-04-2
α-hydroxy-2,5-dihydrocumene

: C₁₇H₁₇N₃O₄

Guidance literature:: Multi-step reaction with 6 steps

1: 61 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 2 h / 0 - 5 °C

2: 86 percent / imidazole / dimethylformamide / 10 h / Ambient temperature

3: 81 percent / Br₂ / CCl₄ / 0 °C

4: 41 percent / DBN / diethyl ether / 4 h / Ambient temperature

5: 87 percent / KF / methanol / 2 h / 0 °C

6: CHCl₃

With 1H-imidazole; potassium fluoride; 2,6-dichloro-benzonitrile; bromine; 3-chloro-benzenecarboperoxoic acid; In methanol; tetrachloromethane; diethyl ether; dichloromethane; chloroform; N,N-dimethyl-formamide;
DOI:10.1021/ja00394a029