C₁₄H₁₁BrN₂O₃

Base Information

• Chemical Name: C₁₄H₁₁BrN₂O₃
• CAS No.: 1315303-28-6
• Molecular Formula: C₁₄H₁₁BrN₂O₃
• Molecular Weight: 335.157
• Mol file: 1315303-28-6.mol

Synonyms:C₁₄H₁₁BrN₂O₃

Chemical Property of C₁₄H₁₁BrN₂O₃

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of C₁₄H₁₁BrN₂O₃

There total 1 articles about C₁₄H₁₁BrN₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

4-methoxy-aniline (104-94-9) + 2-bromo-3-nitrobenzaldehyde (90407-21-9) → C14H11BrN2O3 (1315303-28-6)

Guidance literature:

With acetic acid; at 20 ℃;

DOI:10.1039/c1cc12152a

Reference yield: 82.0%

C14H11BrN2O3 (1315303-28-6) → C14H13BrN2O3 (1315303-29-7)

Guidance literature:

With sodium tetrahydroborate; In ethanol; at 20 ℃; for 6h; Inert atmosphere;

DOI:10.1039/c1cc12152a

Reference yield:

C14H11BrN2O3 (1315303-28-6) → C28H20N4O6Se2 (1315303-34-4)

Guidance literature:

Multi-step reaction with 3 steps

1.1: sodium tetrahydroborate / ethanol / 6 h / 20 °C / Inert atmosphere

2.1: sodium tetrahydroborate / ethanol / 0.5 h / 0 - 20 °C

2.2: 4 h / 20 °C

3.1: bromine / chloroform / 0 °C / Inert atmosphere

3.2: 3 h / 20 °C / Inert atmosphere

With sodium tetrahydroborate; bromine; In ethanol; chloroform;

DOI:10.1039/c1cc12152a

upstream raw materials:

4-methoxy-aniline

2-bromo-3-nitrobenzaldehyde

Downstream raw materials:

C₂₈H₂₀N₄O₆Se₂

C₁₈H₂₂N₂O₃Se

C₁₄H₁₃BrN₂O₃