4-bromo-N-butyrylbenzamide

Base Information

Chemical Name:4-bromo-N-butyrylbenzamide
CAS No.:39549-69-4
Molecular Formula:C₁₁H₁₂BrNO₂
Molecular Weight:270.126
Hs Code.:

Synonyms:4-bromo-N-butyrylbenzamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-bromo-N-butyrylbenzamide

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Technology Process of 4-bromo-N-butyrylbenzamide

There total 2 articles about 4-bromo-N-butyrylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 623-00-7
4-bromobenzenecarbonitrile

: N-butylammonium butyrate

: 698-67-9
p-bromobenzamide

: 39549-69-4
4-bromo-N-butyrylbenzamide

Guidance literature:: N-butylammonium butyrate; With trifluoromethylsulfonic anhydride; at 0 - 20 ℃; for 0.0833333h;

4-bromobenzenecarbonitrile; at 60 ℃; for 1h;

With water; sodium hydrogencarbonate;
DOI:10.1016/j.tetlet.2012.03.121

Reference yield: 80.0%

: 2432-51-1
ethylthioacetic acid methyl ester

: 698-67-9
p-bromobenzamide

: 39549-69-4
4-bromo-N-butyrylbenzamide

Guidance literature:: p-bromobenzamide; With N-Bromosuccinimide; iron(II) chloride; In acetonitrile; at 20 ℃; for 0.0166667h;

ethylthioacetic acid methyl ester; In acetonitrile; at 45 ℃; for 8h;
DOI:10.1002/adsc.200800668