methyl (Z)-3-O-benzyl-5,6-dideoxy-1,2-O-cyclohexylidene-α-D-xylo-hept-5-enofuranuronate

Base Information

Chemical Name:methyl (Z)-3-O-benzyl-5,6-dideoxy-1,2-O-cyclohexylidene-α-D-xylo-hept-5-enofuranuronate
CAS No.:645403-03-8
Molecular Formula:C₂₁H₂₆O₆
Molecular Weight:374.434
Hs Code.:

Synonyms:methyl (Z)-3-O-benzyl-5,6-dideoxy-1,2-O-cyclohexylidene-α-D-xylo-hept-5-enofuranuronate

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Chemical Property of methyl (Z)-3-O-benzyl-5,6-dideoxy-1,2-O-cyclohexylidene-α-D-xylo-hept-5-enofuranuronate

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Technology Process of methyl (Z)-3-O-benzyl-5,6-dideoxy-1,2-O-cyclohexylidene-α-D-xylo-hept-5-enofuranuronate

There total 2 articles about methyl (Z)-3-O-benzyl-5,6-dideoxy-1,2-O-cyclohexylidene-α-D-xylo-hept-5-enofuranuronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: [(methoxycarbonyl)methyl]triphenylphosphorane

: 15354-75-3
3-O-benzyl-1,2-O-cyclohexylidene-α-D-xylo-pentodialdo-1,4-furanose

: 645403-03-8
methyl (Z)-3-O-benzyl-5,6-dideoxy-1,2-O-cyclohexylidene-α-D-xylo-hept-5-enofuranuronate

: 1083324-84-8
methyl (E)-3-O-benzyl-5,6-dideoxy-1,2-O-cyclohexylidene-α-D-xylo-hept-5-enofuranuronate

Guidance literature:: In methanol; at 0 - 20 ℃; for 2h;
DOI:10.1016/j.bmcl.2008.08.093

Reference yield: 83.0%

: 15354-75-3
3-O-benzyl-1,2-O-cyclohexylidene-α-D-xylo-pentodialdo-1,4-furanose

: 21204-67-1,2605-67-6
methyl (triphenylphosphoranylidene)acetate

: 645403-03-8
methyl (Z)-3-O-benzyl-5,6-dideoxy-1,2-O-cyclohexylidene-α-D-xylo-hept-5-enofuranuronate

: 1083324-84-8
methyl (E)-3-O-benzyl-5,6-dideoxy-1,2-O-cyclohexylidene-α-D-xylo-hept-5-enofuranuronate

Guidance literature:: In methanol; at 0 - 20 ℃; for 2h; stereoselective reaction;
DOI:10.1016/j.tet.2009.10.079

Reference yield: 74.0%

: 645403-03-8
methyl (Z)-3-O-benzyl-5,6-dideoxy-1,2-O-cyclohexylidene-α-D-xylo-hept-5-enofuranuronate

: C₁₆H₂₀O₆

: 139534-92-2
(3aS,5R,6S,6aR)-6-Benzyloxy-5-dimethoxymethyl-tetrahydro-furo[3,2-b]furan-2-one

Guidance literature:: methyl (Z)-3-O-benzyl-5,6-dideoxy-1,2-O-cyclohexylidene-α-D-xylo-hept-5-enofuranuronate; With sulfuric acid; In methanol; for 4.5h; Reflux;

With sodium hydrogencarbonate; In methanol; at 35 ℃; for 1h;
DOI:10.1016/j.bmcl.2008.08.093