3-(4-Phenyl-[1, 2, 3]triazol-1-ylmethyl)-benzaldehyde

Base Information

Chemical Name:3-(4-Phenyl-[1, 2, 3]triazol-1-ylmethyl)-benzaldehyde
CAS No.:1267502-78-2
Molecular Formula:C₁₆H₁₃N₃O
Molecular Weight:263.299
Hs Code.:

Synonyms:3-(4-Phenyl-[1, 2, 3]triazol-1-ylmethyl)-benzaldehyde

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Chemical Property of 3-(4-Phenyl-[1, 2, 3]triazol-1-ylmethyl)-benzaldehyde

Chemical Property:

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Technology Process of 3-(4-Phenyl-[1, 2, 3]triazol-1-ylmethyl)-benzaldehyde

There total 6 articles about 3-(4-Phenyl-[1, 2, 3]triazol-1-ylmethyl)-benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 1267502-77-1
[3-(4-phenyl-[1,2,3]triazol-1-ylmethyl)-phenyl]-methanol

: 1267502-78-2
3-(4-Phenyl-[1, 2, 3]triazol-1-ylmethyl)-benzaldehyde

Guidance literature:: With sodium acetate; pyridinium chlorochromate; In dichloromethane; at 25 ℃; for 2h;

Reference yield:

: 6515-58-8
3-bromomethylbenzoic acid

: 1267502-78-2
3-(4-Phenyl-[1, 2, 3]triazol-1-ylmethyl)-benzaldehyde

Guidance literature:: Multi-step reaction with 5 steps

1: thionyl chloride / 1 h / 25 °C / Reflux

2: sodium azide / N,N-dimethyl-formamide / 3 h / 80 °C

3: N-ethyl-N,N-diisopropylamine / copper(l) iodide; sodium L-ascorbate / N,N-dimethyl-formamide / 12 h / 25 °C

4: lithium aluminium tetrahydride / tetrahydrofuran / 1 h

5: sodium acetate; pyridinium chlorochromate / dichloromethane / 2 h / 25 °C

With lithium aluminium tetrahydride; thionyl chloride; sodium azide; sodium acetate; N-ethyl-N,N-diisopropylamine; pyridinium chlorochromate; copper(l) iodide; sodium L-ascorbate; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 99-04-7
m-Toluic acid

: 1267502-78-2
3-(4-Phenyl-[1, 2, 3]triazol-1-ylmethyl)-benzaldehyde

Guidance literature:: Multi-step reaction with 6 steps

1: N-Bromosuccinimide / 2,2'-azobis(isobutyronitrile) / tetrachloromethane / 3 h / 25 °C / Reflux

2: thionyl chloride / 1 h / 25 °C / Reflux

3: sodium azide / N,N-dimethyl-formamide / 3 h / 80 °C

4: N-ethyl-N,N-diisopropylamine / copper(l) iodide; sodium L-ascorbate / N,N-dimethyl-formamide / 12 h / 25 °C

5: lithium aluminium tetrahydride / tetrahydrofuran / 1 h

6: sodium acetate; pyridinium chlorochromate / dichloromethane / 2 h / 25 °C

With N-Bromosuccinimide; lithium aluminium tetrahydride; thionyl chloride; sodium azide; sodium acetate; N-ethyl-N,N-diisopropylamine; pyridinium chlorochromate; copper(l) iodide; 2,2'-azobis(isobutyronitrile); sodium L-ascorbate; In tetrahydrofuran; tetrachloromethane; dichloromethane; N,N-dimethyl-formamide;