N,N'-di-n-octyl-2-chloro-6-[(4-tert-butylphenyl)amino]-1,4,5,8-naphthalenetetracarboxylic acid diimide

Base Information

Chemical Name:N,N'-di-n-octyl-2-chloro-6-[(4-tert-butylphenyl)amino]-1,4,5,8-naphthalenetetracarboxylic acid diimide
CAS No.:914455-64-4
Molecular Formula:C₄₀H₅₀ClN₃O₄
Molecular Weight:672.308
Hs Code.:

Synonyms:N,N'-di-n-octyl-2-chloro-6-[(4-tert-butylphenyl)amino]-1,4,5,8-naphthalenetetracarboxylic acid diimide

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Chemical Property of N,N'-di-n-octyl-2-chloro-6-[(4-tert-butylphenyl)amino]-1,4,5,8-naphthalenetetracarboxylic acid diimide

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Technology Process of N,N'-di-n-octyl-2-chloro-6-[(4-tert-butylphenyl)amino]-1,4,5,8-naphthalenetetracarboxylic acid diimide

There total 4 articles about N,N'-di-n-octyl-2-chloro-6-[(4-tert-butylphenyl)amino]-1,4,5,8-naphthalenetetracarboxylic acid diimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 510774-95-5
N,N'-di-(n-octyl)-2,6-dichloro-1,4,5,8-naphthalenetetracarboxylic acid diimide

: 769-92-6
4-tert-Butylaniline

: 914455-64-4
N,N'-di-n-octyl-2-chloro-6-[(4-tert-butylphenyl)amino]-1,4,5,8-naphthalenetetracarboxylic acid diimide

Guidance literature:: With N-ethyl-N,N-diisopropylamine; at 140 ℃; for 1h;
DOI:10.1021/jo0612269

Reference yield:

: 32692-38-9
1,3,4,5,6,8,9,10-octachloro-4,5,9,10-tetrahydropyrene

: 914455-64-4
N,N'-di-n-octyl-2-chloro-6-[(4-tert-butylphenyl)amino]-1,4,5,8-naphthalenetetracarboxylic acid diimide

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium hydroxide / ethanol / 5 h / Heating

1.2: 3.33 g / fuming nitric acid / -5 - 5 °C

2.1: 49 percent / sulfuric acid; fuming nitric acid / 100 - 130 °C

3.1: 70 percent / acetic acid / 0.17 h / Heating

4.1: 97 percent / ethyldiisopropylamine / 1 h / 140 °C

With potassium hydroxide; sulfuric acid; nitric acid; acetic acid; N-ethyl-N,N-diisopropylamine; In ethanol;
DOI:10.1021/jo0612269

Reference yield:

: 5355-83-9
3,5,8,10-tetrachloropyrene-1,6-quinone

: 914455-64-4
N,N'-di-n-octyl-2-chloro-6-[(4-tert-butylphenyl)amino]-1,4,5,8-naphthalenetetracarboxylic acid diimide

Guidance literature:: Multi-step reaction with 3 steps

1: 49 percent / sulfuric acid; fuming nitric acid / 100 - 130 °C

2: 70 percent / acetic acid / 0.17 h / Heating

3: 97 percent / ethyldiisopropylamine / 1 h / 140 °C

With sulfuric acid; nitric acid; acetic acid; N-ethyl-N,N-diisopropylamine;
DOI:10.1021/jo0612269