2-n-butyl-1-(4-carbomethoxy-3-methoxymethoxyphenyl)-methyl-1H-imidazol-5-carboxaldehyde

Base Information

Chemical Name:2-n-butyl-1-(4-carbomethoxy-3-methoxymethoxyphenyl)-methyl-1H-imidazol-5-carboxaldehyde
CAS No.:149543-79-3
Molecular Formula:C₁₉H₂₄N₂O₅
Molecular Weight:360.41
Hs Code.:

Synonyms:2-n-butyl-1-(4-carbomethoxy-3-methoxymethoxyphenyl)-methyl-1H-imidazol-5-carboxaldehyde

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Chemical Property of 2-n-butyl-1-(4-carbomethoxy-3-methoxymethoxyphenyl)-methyl-1H-imidazol-5-carboxaldehyde

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Technology Process of 2-n-butyl-1-(4-carbomethoxy-3-methoxymethoxyphenyl)-methyl-1H-imidazol-5-carboxaldehyde

There total 3 articles about 2-n-butyl-1-(4-carbomethoxy-3-methoxymethoxyphenyl)-methyl-1H-imidazol-5-carboxaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 149543-78-2
2-n-butyl-1-(4-carbomethoxy-3-methoxymethoxyphenyl)methyl-4-chloro-1H-imidazol-5-carboxaldehyde

: 149543-79-3
2-n-butyl-1-(4-carbomethoxy-3-methoxymethoxyphenyl)-methyl-1H-imidazol-5-carboxaldehyde

Guidance literature:: With manganese(IV) oxide; hydrogen; potassium acetate; palladium on activated charcoal; Multistep reaction; 1.) MeOH, 40 psi, 1.25 h, 2.) CH₂Cl₂, reflux;
DOI:10.1021/jm00065a011

Reference yield:

: 83857-96-9
2-n-butyl-4-chloro-1H-imidazol-5-carboxaldehyde

: 149543-79-3
2-n-butyl-1-(4-carbomethoxy-3-methoxymethoxyphenyl)-methyl-1H-imidazol-5-carboxaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 1 h / 70 °C

2: manganese(IV) oxide; hydrogen; potassium acetate / palladium on activated charcoal / 1.) MeOH, 40 psi, 1.25 h, 2.) CH₂Cl₂, reflux

With manganese(IV) oxide; hydrogen; potassium acetate; potassium carbonate; palladium on activated charcoal; In N,N-dimethyl-formamide;
DOI:10.1021/jm00065a011

Reference yield:

: 149543-77-1
methyl 4-bromomethyl-2-methoxymethoxybenzoate

: 149543-79-3
2-n-butyl-1-(4-carbomethoxy-3-methoxymethoxyphenyl)-methyl-1H-imidazol-5-carboxaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 1 h / 70 °C

2: manganese(IV) oxide; hydrogen; potassium acetate / palladium on activated charcoal / 1.) MeOH, 40 psi, 1.25 h, 2.) CH₂Cl₂, reflux

With manganese(IV) oxide; hydrogen; potassium acetate; potassium carbonate; palladium on activated charcoal; In N,N-dimethyl-formamide;
DOI:10.1021/jm00065a011