N-methoxy-1-tosylmethanimidoyl cyanide

Base Information

Chemical Name:N-methoxy-1-tosylmethanimidoyl cyanide
CAS No.:74754-99-7
Molecular Formula:C₁₀H₁₀N₂O₃S
Molecular Weight:238.267
Hs Code.:

Synonyms:N-methoxy-1-tosylmethanimidoyl cyanide

Suppliers and Price of N-methoxy-1-tosylmethanimidoyl cyanide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-methoxy-1-tosylmethanimidoyl cyanide

Chemical Property:

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Technology Process of N-methoxy-1-tosylmethanimidoyl cyanide

There total 3 articles about N-methoxy-1-tosylmethanimidoyl cyanide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 175201-58-8
C₉H₈N₂O₃S

: 77-78-1
dimethyl sulfate

: 74754-99-7
N-methoxy-1-tosylmethanimidoyl cyanide

Guidance literature:: With potassium carbonate; In tetrahydrofuran; at 20 ℃; for 3h;
DOI:10.1016/j.tet.2013.09.051

Reference yield:

: 5697-44-9
p-tolylsulfonylmethyl isocyanide

: 74754-99-7
N-methoxy-1-tosylmethanimidoyl cyanide

Guidance literature:: Multi-step reaction with 2 steps

1: isopentyl nitrite; sodium ethanolate / ethanol / 24 h / 20 °C

2: potassium carbonate / tetrahydrofuran / 3 h / 20 °C

With sodium ethanolate; potassium carbonate; isopentyl nitrite; In tetrahydrofuran; ethanol;
DOI:10.1016/j.tet.2013.09.051