dibenzyl phthalimidomethylphosphonate

Base Information

Chemical Name:dibenzyl phthalimidomethylphosphonate
CAS No.:96914-74-8
Molecular Formula:C₂₃H₂₀NO₅P
Molecular Weight:421.389
Hs Code.:

Synonyms:dibenzyl phthalimidomethylphosphonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dibenzyl phthalimidomethylphosphonate

Chemical Property:

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Technology Process of dibenzyl phthalimidomethylphosphonate

There total 2 articles about dibenzyl phthalimidomethylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 5332-26-3
N-(bromomethyl)phtalimide

: 17176-77-1
Dibenzyl phosphite

: 96914-74-8
dibenzyl phthalimidomethylphosphonate

Guidance literature:: Dibenzyl phosphite; With sodium hydride; In tetrahydrofuran; mineral oil; at -15 ℃; for 0.5h;

N-(bromomethyl)phtalimide; In tetrahydrofuran; mineral oil; at -15 - 20 ℃; for 16.1667h;
DOI:10.1021/ol300664d

Reference yield:

: 5332-26-3
N-(bromomethyl)phtalimide

: 56522-04-4
dibenzylphosphine

: 96914-74-8
dibenzyl phthalimidomethylphosphonate

Guidance literature:: With sodium hydride; Yield given. Multistep reaction; 1.) THF, -15 deg C, 15 min, 2.) THF, RT, 16 h;
DOI:10.1021/jm00147a015

Reference yield: 11.0%

: 96914-74-8
dibenzyl phthalimidomethylphosphonate

: Pro-Phe-pCMA

: 460053-76-3
Pht=GlyΨ(PO2Bn-N)Pro-Phe-pCMA

Guidance literature:: dibenzyl phthalimidomethylphosphonate; With phosphorus pentachloride; In tetrachloromethane; for 7h; Heating;

Pro-Phe-pCMA; With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; at 20 ℃; Further stages.;
DOI:10.1021/jm020865i