C₃₇H₄₄BrN₃O₁₀

Base Information

Chemical Name:C₃₇H₄₄BrN₃O₁₀
CAS No.:1310875-44-5
Molecular Formula:C₃₇H₄₄BrN₃O₁₀
Molecular Weight:770.674
Hs Code.:

C<sub>37</sub>H<sub>44</sub>BrN<sub>3</sub>O<sub>10</sub>

Synonyms:C₃₇H₄₄BrN₃O₁₀

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Chemical Property of C₃₇H₄₄BrN₃O₁₀

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Technology Process of C₃₇H₄₄BrN₃O₁₀

There total 6 articles about C₃₇H₄₄BrN₃O₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1310875-43-4
C₄₉H₇₂BrN₃O₁₀Si₂

: 1310875-44-5
C₃₇H₄₄BrN₃O₁₀

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 ℃; for 1h;
DOI:10.1021/jo200758r

Reference yield:

: 67561-03-9
N-benzyloxycarbonylglycinal

: 1310875-44-5
C₃₇H₄₄BrN₃O₁₀

Guidance literature:: Multi-step reaction with 6 steps

1: acetic acid / dichloromethane; 2,2,2-trifluoroethanol / 10 h / 0 °C / Inert atmosphere; Molecular sieve

2: 1H-imidazole / N,N-dimethyl-formamide / 48 h / 20 °C / Inert atmosphere

3: bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; triethylamine / dichloromethane / 72 h / 20 °C / Cooling with ice

4: formic acid / tetrahydrofuran; water / 10 h / 20 °C

5: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 2 h / 20 °C

6: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 0 °C

With 1H-imidazole; formic acid; tetrabutyl ammonium fluoride; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; sodium hydrogencarbonate; Dess-Martin periodane; acetic acid; triethylamine; In tetrahydrofuran; dichloromethane; 2,2,2-trifluoroethanol; water; N,N-dimethyl-formamide; 1: Pictet-Spengler cyclisation;
DOI:10.1021/jo200758r

Reference yield:

: 1310875-39-8
benzyl ((1R,3S)-8-hydroxy-3-(hydroxymethyl)-7-methoxy-6-methyl-1,2,3,4-tetrahydroisoquinolin-1-yl)methylcarbamate

: 1310875-44-5
C₃₇H₄₄BrN₃O₁₀

Guidance literature:: Multi-step reaction with 5 steps

1: 1H-imidazole / N,N-dimethyl-formamide / 48 h / 20 °C / Inert atmosphere

2: bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; triethylamine / dichloromethane / 72 h / 20 °C / Cooling with ice

3: formic acid / tetrahydrofuran; water / 10 h / 20 °C

4: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 2 h / 20 °C

5: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 0 °C

With 1H-imidazole; formic acid; tetrabutyl ammonium fluoride; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; sodium hydrogencarbonate; Dess-Martin periodane; triethylamine; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/jo200758r