-(3al,7l,7al)-1,2,3,3a,7,7a-hexahydro-6-methyl-7-phenylcyclopent<1,2>oxazine N-oxide

Base Information

Chemical Name:-(3al,7l,7al)-1,2,3,3a,7,7a-hexahydro-6-methyl-7-phenylcyclopent<1,2>oxazine N-oxide
CAS No.:142840-09-3
Molecular Formula:C₁₄H₁₇NO₂
Molecular Weight:231.294
Hs Code.:

<R,S>-(3al,7l,7al)-1,2,3,3a,7,7a-hexahydro-6-methyl-7-phenylcyclopent<e><1,2>oxazine N-oxide

Synonyms:-(3al,7l,7al)-1,2,3,3a,7,7a-hexahydro-6-methyl-7-phenylcyclopent<1,2>oxazine N-oxide

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Chemical Property of -(3al,7l,7al)-1,2,3,3a,7,7a-hexahydro-6-methyl-7-phenylcyclopent<1,2>oxazine N-oxide

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Technology Process of -(3al,7l,7al)-1,2,3,3a,7,7a-hexahydro-6-methyl-7-phenylcyclopent<1,2>oxazine N-oxide

There total 2 articles about -(3al,7l,7al)-1,2,3,3a,7,7a-hexahydro-6-methyl-7-phenylcyclopent<1,2>oxazine N-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 705-60-2
(2-nitroprop-1-enyl)benzene

: 142-29-0
cyclopentene

: 142840-09-3
-(3al,7l,7al)-1,2,3,3a,7,7a-hexahydro-6-methyl-7-phenylcyclopent<1,2>oxazine N-oxide

Guidance literature:: With tin(IV) chloride; In dichloromethane; at -78 ℃; for 0.75h; Product distribution; Mechanism; other nitroalkenes and cycloalkenes; diastereoselectivity; velocity;
DOI:10.1021/jo00044a029

Reference yield: 75.0%

: 705-60-2,18315-84-9,58321-79-2
1-phenyl-2-nitroprop-1-ene

: 142-29-0
cyclopentene

: 142840-09-3
-(3al,7l,7al)-1,2,3,3a,7,7a-hexahydro-6-methyl-7-phenylcyclopent<1,2>oxazine N-oxide

Guidance literature:: With tin(IV) chloride;
DOI:10.1055/s-2006-958930

Reference yield: 50.0%

: 142840-09-3
-(3al,7l,7al)-1,2,3,3a,7,7a-hexahydro-6-methyl-7-phenylcyclopent<1,2>oxazine N-oxide

: (4RS,4aSR,7aSR)-3-(bromomethyl)-4-phenyl-4,4a,5,6,7,7a-hexahydrocyclopenta[e][1,2]oxazine

Guidance literature:: -(3al,7l,7al)-1,2,3,3a,7,7a-hexahydro-6-methyl-7-phenylcyclopent<1,2>oxazine N-oxide; With trimethylsilyl bromide; triethylamine; In dichloromethane; at -80 ℃; for 1h;

With acetonitrile; In dichloromethane; at -30 ℃; for 3h; Further stages.;
DOI:10.1055/s-2006-958930