5-(4-chlorophenyl)-4,5-dihydro-3-(4-methoxyphenyl)-N-phenyl-1H-pyrazole-1-carbothioamide

Base Information

Chemical Name:5-(4-chlorophenyl)-4,5-dihydro-3-(4-methoxyphenyl)-N-phenyl-1H-pyrazole-1-carbothioamide
CAS No.:75758-29-1
Molecular Formula:C₂₃H₂₀ClN₃OS
Molecular Weight:421.95
Hs Code.:

Synonyms:5-(4-chlorophenyl)-4,5-dihydro-3-(4-methoxyphenyl)-N-phenyl-1H-pyrazole-1-carbothioamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-(4-chlorophenyl)-4,5-dihydro-3-(4-methoxyphenyl)-N-phenyl-1H-pyrazole-1-carbothioamide

Chemical Property:

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Technology Process of 5-(4-chlorophenyl)-4,5-dihydro-3-(4-methoxyphenyl)-N-phenyl-1H-pyrazole-1-carbothioamide

There total 3 articles about 5-(4-chlorophenyl)-4,5-dihydro-3-(4-methoxyphenyl)-N-phenyl-1H-pyrazole-1-carbothioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 75745-48-1
5-(4-chlorophenyl)-3-(4-methoxyphenyl)-4,5-dihydro-1H-pyrazole

: 103-72-0
phenyl isothiocyanate

: 75758-29-1
5-(4-chlorophenyl)-4,5-dihydro-3-(4-methoxyphenyl)-N-phenyl-1H-pyrazole-1-carbothioamide

Guidance literature:: triethylamine; In diethyl ether; for 4h; Ambient temperature;

Reference yield:

: 6552-68-7
4-chloro-4'-methoxy-chalcone

: 75758-29-1
5-(4-chlorophenyl)-4,5-dihydro-3-(4-methoxyphenyl)-N-phenyl-1H-pyrazole-1-carbothioamide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / ethanol / 2 h / Reflux

2: chloroform / Reflux

With hydrazine hydrate; In ethanol; chloroform;
DOI:10.1002/cbdv.201400143

Reference yield:

: 104-88-1
4-chlorobenzaldehyde

: 75758-29-1
5-(4-chlorophenyl)-4,5-dihydro-3-(4-methoxyphenyl)-N-phenyl-1H-pyrazole-1-carbothioamide

Guidance literature:: Multi-step reaction with 3 steps

1: potassium hydroxide / ethanol; water / 4 h / 20 °C / Cooling

2: hydrazine hydrate / ethanol / 2 h / Reflux

3: chloroform / Reflux

With hydrazine hydrate; potassium hydroxide; In ethanol; chloroform; water; 1: |Claisen-Schmidt Condensation;
DOI:10.1002/cbdv.201400143