5-(4-bromophenyl)-3-(4-chlorophenyl)-1H-[1,3]oxazino[4,5-c]quinolin-1-one

Base Information

• Chemical Name: 5-(4-bromophenyl)-3-(4-chlorophenyl)-1H-[1,3]oxazino[4,5-c]quinolin-1-one
• CAS No.: 936024-63-4
• Molecular Formula: C₂₃H₁₂BrClN₂O₂
• Molecular Weight: 463.717

Synonyms:5-(4-bromophenyl)-3-(4-chlorophenyl)-1H-[1,3]oxazino[4,5-c]quinolin-1-one

Chemical Property of 5-(4-bromophenyl)-3-(4-chlorophenyl)-1H-[1,3]oxazino[4,5-c]quinolin-1-one

Chemical Property:

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Technology Process of 5-(4-bromophenyl)-3-(4-chlorophenyl)-1H-[1,3]oxazino[4,5-c]quinolin-1-one

There total 4 articles about 5-(4-bromophenyl)-3-(4-chlorophenyl)-1H-[1,3]oxazino[4,5-c]quinolin-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

α-amino-4-bromoacetophenone hydrochloride (5467-72-1) → 5-(4-bromophenyl)-3-(4-chlorophenyl)-1H-[1,3]oxazino[4,5-c]quinolin-1-one (936024-63-4)

Guidance literature:

Multi-step reaction with 3 steps

1: NaOH / ethanol; tetrahydrofuran; H₂O / 0.5 h / Heating

2: pyridine / 12 h / 20 °C

3: acetic anhydride / 5 h / Heating

With pyridine; sodium hydroxide; acetic anhydride; In tetrahydrofuran; ethanol; water;

DOI:10.1016/j.ejmech.2006.10.008

Reference yield:

indole-2,3-dione (91-56-5,1186480-61-4,84788-92-1) → 5-(4-bromophenyl)-3-(4-chlorophenyl)-1H-[1,3]oxazino[4,5-c]quinolin-1-one (936024-63-4)

Guidance literature:

Multi-step reaction with 3 steps

1: NaOH / ethanol; tetrahydrofuran; H₂O / 0.5 h / Heating

2: pyridine / 12 h / 20 °C

3: acetic anhydride / 5 h / Heating

With pyridine; sodium hydroxide; acetic anhydride; In tetrahydrofuran; ethanol; water;

DOI:10.1016/j.ejmech.2006.10.008

Reference yield:

2-(4-bromo-phenyl)-3-(4-chloro-benzoylamino)-quinoline-4-carboxylic acid → 5-(4-bromophenyl)-3-(4-chlorophenyl)-1H-[1,3]oxazino[4,5-c]quinolin-1-one (936024-63-4)

Guidance literature:

With acetic anhydride; for 5h; Heating;

DOI:10.1016/j.ejmech.2006.10.008

upstream raw materials:

3-amino-2-(4-bromo-phenyl)-quinoline-4-carboxylic acid

α-amino-4-bromoacetophenone hydrochloride

indole-2,3-dione

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