Methyl-2-aminomethyl-5-benzyloxycarbonyl-4-(2-methoxycarbonylethyl)pyrrol-3-propionat hydrochlorid

Base Information

Chemical Name:Methyl-2-aminomethyl-5-benzyloxycarbonyl-4-(2-methoxycarbonylethyl)pyrrol-3-propionat hydrochlorid
CAS No.:73870-09-4
Molecular Formula:C₂₁H₂₆N₂O₆*ClH
Molecular Weight:438.908
Hs Code.:

Synonyms:Methyl-2-aminomethyl-5-benzyloxycarbonyl-4-(2-methoxycarbonylethyl)pyrrol-3-propionat hydrochlorid

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Chemical Property of Methyl-2-aminomethyl-5-benzyloxycarbonyl-4-(2-methoxycarbonylethyl)pyrrol-3-propionat hydrochlorid

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Technology Process of Methyl-2-aminomethyl-5-benzyloxycarbonyl-4-(2-methoxycarbonylethyl)pyrrol-3-propionat hydrochlorid

There total 8 articles about Methyl-2-aminomethyl-5-benzyloxycarbonyl-4-(2-methoxycarbonylethyl)pyrrol-3-propionat hydrochlorid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 73870-08-3
Methyl-5-benzyloxycarbonyl-4-(2-methoxycarbonylethyl)-2-hydroxyiminomethylpyrrol-3-propionat

: 73870-09-4
Methyl-2-aminomethyl-5-benzyloxycarbonyl-4-(2-methoxycarbonylethyl)pyrrol-3-propionat hydrochlorid

Guidance literature:: With hydrogenchloride; zinc; In methanol;

Reference yield:

: 58950-57-5
3-(2-ethoxycarbonylethyl)-4-formyl-5-methylpyrrole-2-carboxylate

: 73870-09-4
Methyl-2-aminomethyl-5-benzyloxycarbonyl-4-(2-methoxycarbonylethyl)pyrrol-3-propionat hydrochlorid

Guidance literature:: Multi-step reaction with 8 steps

1: 83 percent / pyridine; various solvent(s) / 5 h / 90 - 100 °C

2: 71 percent / 1) H₂ / 1) Raney - Ni / 1) MeOH, 2) 60 deg C, 30 min

3: 93 percent / HCl / 24 h / 25 °C

4: 82 percent / Na / 1) steam bath, 1 h, 2) 10 Torr, 3 h

5: 92 percent / HCl / 24 h / 25 °C

6: 1) SO₂Cl₂, 3) NaOAc/H₂O / 1) CH₂Cl₂, 0 deg C, 15 min, 2) 20 deg C, 75 min, 3) steam bath, 10 min, water

7: 86 percent / NH₂OH*HCl, NaOEt / H₂O / 1 h / Heating

8: 84 percent / HCl/Zn / methanol

With hydrogenchloride; sulfuryl dichloride; hydroxylamine hydrochloride; water; hydrogen; sodium ethanolate; sodium acetate; sodium; zinc; nickel; In pyridine; methanol; water;

Reference yield:

: 73870-02-7
Ethyl-3-(2-carboxyvinyl)-5-ethoxycarbonyl-2-methylpyrrol-4-propionat

: 73870-09-4
Methyl-2-aminomethyl-5-benzyloxycarbonyl-4-(2-methoxycarbonylethyl)pyrrol-3-propionat hydrochlorid

Guidance literature:: Multi-step reaction with 7 steps

1: 71 percent / 1) H₂ / 1) Raney - Ni / 1) MeOH, 2) 60 deg C, 30 min

2: 93 percent / HCl / 24 h / 25 °C

3: 82 percent / Na / 1) steam bath, 1 h, 2) 10 Torr, 3 h

4: 92 percent / HCl / 24 h / 25 °C

5: 1) SO₂Cl₂, 3) NaOAc/H₂O / 1) CH₂Cl₂, 0 deg C, 15 min, 2) 20 deg C, 75 min, 3) steam bath, 10 min, water

6: 86 percent / NH₂OH*HCl, NaOEt / H₂O / 1 h / Heating

7: 84 percent / HCl/Zn / methanol

With hydrogenchloride; sulfuryl dichloride; hydroxylamine hydrochloride; water; hydrogen; sodium ethanolate; sodium acetate; sodium; zinc; nickel; In methanol; water;